GC/MS analysis report for sample AE06411, May 3 2002

NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\MSDCHEM\l\DATA\020409\6411.D Vial: 15 Acq On : 10 Apr 2002 4:11 am Operator: McLean Sample : 3/18 Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e Quant Method : C:\MSDCHEM\1...\SCANAPR0902.M (Chemstation Integrator) Title : Method 508 GC/MS Scan Library : C:\DATABASE\nist98.1 ********************************************************************* Peak Number 3 Acetic acid, 3-[1,3]dioxola... Concentration Rank 1 R.T. EstConc Area Relative to ISTD R.T.

5.55 1.48 ug/l 1074920 1,4-Dichlorobenzene-d4 10.67 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Acetic acid, 3-[1,3]dioxolan-2-y... 174 C8H14O4 1000186-02-3 45 2 3-Pentanol,. 3-methyl- 102 C6H14O 000077-74-7 36 3 Pentane, 3-methoxy- 102 C6H14O 036839-67-5 9 4 Silane, tetramethyl- 88 C4H12Si 000075-76-3 9 Abundance Scan 420 (5.547 min): 6411 .D (-417) (-) m/z 73.10. 100.00% 7|3

553 43 5.20 5.40 5.60 5.80 ,,l,l 87 ................. m/z 43.10 29.78% Tl/Z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 Abundance #25344: Acetic acid, 3-[1,3]dioxolan-2-ylpropyl ester 7(3

5000 5.20 5.40 5.60 5.80 43 m/z 45.10 12.25% 27 ,. .1 55 87 113 131 174 Tife-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 Abundance #114875: 3-Pentanol, 3-methyl- 7)3

5.20 5.40 5.60 5.80 5000 m/z 41.10 11.58% 55 27 87 15 II, 37ill .... ........... 63 I ,1....... ... .. ..... ■n/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 Abundance #25472: Pentane, 3-methoxy- 7(3 T' 5.20 5.40 5.60 5.80 m/z 71.10 7.35% 5O00 45

29 55 1,1. 371 ,1 -p i l l 1111 I j I 11 .1 101 '"'I nfe-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 5.20 5.40 5.60 5.80

6411.D SCANAPR0902.M Thu May 02 14:17:33 2002 Page 5

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