GCMS analysis results for sample AE08429, May 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\MSDCHEM\l\DATA\020419\08429.D Vial: 16 Acq On : 19 Apr 2002 10:54 pm Operator: Nefliu Sample : sample Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: rteint.e Quant Method : C:\MSDCHEM\1\METHODS\SCAN020418.M (Chemstation Integrator) Title : Method 508 GC/MS Scan Library : C:\DATABASE\nist98.1 ********************************************************************* Peak Number 3 Acetic acid, 3-[1,3]dioxola... Concentration Rank 4

R.T. EstConc Area Relative to ISTD R.T.

6.11 0.39 ug/1 528838 1,4-Dichlorobenzene-d4 11.38 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Acetic acid, 3-[1,3]dioxolan-2-y... 174 C8H14O4 1000186-02-3 50 2 Butane, 2-methoxy-2-methyl- 102 C6H140 000994-05-8 38 3 3-Pentanol, 3-methyl- 102 C6H140 000077-74-7 28 4 3-Pentanol, 3-methyl- 102 C6H140 000077-74-7 9 Abundance Scan 516 (6.111. min): 08429.D (-512) (-) m/z 73.10 100.00% 73

5000 43

87 5.80 6.00 6.20 6.40

m/z-> 1 151.59... ■11'1 ■ ■ ।। ■ -T 103 111" ■ 111 ri I " 1111 " rl 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 11TT m/z 43.20 27.07% Abundance #25344: Acetic acid, 3-[1,3]dioxolan-2-ylpropyl ester 73

5000 5.80 6.00 6.20 6.40 43 m/z 45.10 13.73% 27 55 87 113 ..... 7’1 AI..... ’I’’n ■ i " ■ ■ i' " 11' ITu’I——I—O0—013000100"T1IpITDTT 131 174 I n/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 Abundance #25351: Butane, 2-methoxy-2-methyl- 73 —AAAMAAM 5.80 6.00 6.20 6.40 5000 m/z 71.00 10.37% 43 55 87 29

lz-> ml TTTTITTTIUTTTTTTTPICTITTPTTTTTTTT 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 Abundance #114875: 3-Pentanol, 3-methyl- 73 *T ** fn-i 5.80 6.00 6.20 6.40 m/ z 41.10 6.33%

5000

27 45 55 63 , 87 —154 137.7.., -TPPmmmmPPTTTTTTTTTTT i1 ■ ■ ■ ।1 44 .... r Mmm Tl/Z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 5.80 6.00 6.20 6.40

08429.D SCAN020418.M Thu May 02 15:38:02 2002 Page 5

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