GCMS results for sample AE07766, Apr 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\MSDCHEM\1\DATA\020415\07766.D Vial : 28 Acq On : 16 Apr 2002 8:51 am Operator: Nefliu Sample : sample Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e

Quant Method C:\MSDCHEM\1\METHODS\041202SCAN.M (Chemstation Integrator) Title 508 Modified GC/MS scan Library C:\DATABASE\NIST98.L ********************************************************************* Peak Number 3 Acetic acid, 3- [1,3]dioxola. . . Concentration Rank 5

R.T. EstConc Area Relative to ISTD R.T.

5.96 0.38 ug/L 250960 1,4-Dichlorobenzene-d4 9.99

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Acetic acid, 3-[1,3]dioxolan-2-y. . . 174 C8H14O4 1000186-02-3 36 2 1-Butanamine, 3-methyl- 87 C5H13N 000107-85-7 9 3 1-Pentanamine 87 C5H13N 000110-58-7 9 4 3-Pentanol, 3-methyl-_______________ 102 C6H140 000077-74-7 9 Abundance Scan 491 (5 964 min). 07766 D (-483) (-) m/z 73.30 100.00% 73

5000 43

87 5tO 5 80 6.00 6.20 640 0- ........ ................. ................. , +TUUmmmmmmTWTITITTLT m/ z 43.30 27.60% Tl/Z--> 0 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 Abundance #25344 Acetic acid, 3-[1,3]dioxolan-2-ylpropyl ester 73

5000 560 5 80 N... 6.00 6.20 6 40 43 m/ z 45.30 10.71% 27 87 113 A 55 131 174 0- mmmTTT 1 —TI TTT n/z-> 0 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 Abundance #670 1-Butanamine, 3-methyl- 33

5 60 5.80 6 00 6 20 640 5000 m/z 41.30 10.63%

2 41 55 70 78 87 0- ■1' i ■ ■■ >I ‘11 ITl 11 "'111" " 11'" i "''' i11 " i" " i ‘ " 11 ’ " 1 r 11' r 11 ’ i" " r'1 r i111111' n/z-> Abundance 0 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180

30 #108145: 1-Pentanamine A5.60 5.80 6.00 6.20 6.40 m/ z 71.30 7.03%

5000

41 55 0 ..... I 1111,1441799 69 79 87 i " i1 ........ Tl/Z--> 0 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 5 60 5 80 6 00 6 20 6.40

07766.D 041202SCAN.M Tue Apr 16 13:42:02 2002 Page 6

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