GC/MS analysis report for sample AE06411, May 3 2002

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Library Search Compound Report

Data File : C:\MSDCHEM\l\DATA\020409\6411.D Vial: 15 Acg On : 10 Apr 2002 4:11 am Operator: McLean Sample : 3/18 Inst : Instrumen Mise : Multiplr: 1.00 MS Integration Params: LSCINT.e

Quant Method : C: \MSDCHEM\1. . .\SC7\NAPR0902 .M (Chemstation Integrator) Title : Method 508 GC/MS Scan Library : C:\DATABASE\nist98.1 ********************************************************************* Peak Number 2 Hydrogen azide Concentration Rank 3 R.T. EstConc Area Relative to ISTD R.T.

3.42 0.21 ug/1 155390 1,4-Dichlorobenzene-d4 10.67 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Hydrogen azide 43 HN3 007782-79-8 1 2 Isobutane 58 C4H10 000075-28-5 1 3 Isobutane 58 C4H10 000075-28-5 1 4 Phenol, 2-(1-methylpropyl)-4,6-d... 282 C12H14N2O6 002813-95-8 1 Abundance Scan 58 (3.420 min): 6411 .D (-53) {-) pm/z 43.10 100.00% 43

8000 I 6000

4000 320 3.40 3.60 3.80 ......... • 40 __________ m/z 40.10 34.44% ' I'''' I'''' I'''' I'''' I'''' I'' ‘' I'''' I'''' I'' ' I ‘' I'''' I'''' I'''' I ‘ •n/z-> 0 5 10 15 20 25 30 35 40 45 50 55 60 65 Abundance #3862: Hydrogen azide 40

5000 15 28 3.20 3.40 3.60 3.80

I I'''' I'''' I'''' I'' ' ’ I' 0 5 10 15 20 25 30 35 40 45 50 55 60 65 Abundance #109242; Isobutane 4(3

5000 27 39 15

■n/z-> 0 2 5 . ...... .lipQ.. 10 15 20 25 30 35 .40 w.....45 50 55 60 65 Abundance #109241; Isobutane 40

5000 27 39 1 12 19 ' I'' ‘' I'''' I' ................. ■n/z-> 0 5 10 15 20 25 30 35 40 45 50 55 60 65

6411.D SCANAPR0902.M Thu May 02 14:17:31 2002 Page 4

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