GCMS analysis results, sample AE07511, April 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File C:\MSDCHEM\l\DATA\020404\07511.D Vial: 7 Acq On 4 Apr 2002 12:34 pm Operator: Nefliu Sample sample Inst Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e

Quant Method : C:\MSDCHEM\1\METHODS\SCAN020403.M (Chemstation Integrator) Title : Method 508 GC/MS Scan Library : C:\DATABASE\nist98.1 Peak Number 3 Hydrogen azide Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T. 3.42 0.19 ug/1 140029 1,4-Dichlorobenzene-d4 10.66 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Hydrogen azide 43 HN3 007782-79-8 1 2 Isobutane 58 C4H10 000075-28-5 1 3 Isobutane 58 C4H10 000075-28-5 1 4 Phenol, 2-(1-methylpropyl)-4,6-d... 282 C12H14N2O6 002813-95-8 1 Abundance Scan 59 (3.426 min): 07511 D (-53) (-) ”m/ z 43.10 100.00% 43

5000

40 320 3.40 3.60 3.80 o1 ■ ■ । ■ 11 । । -111111 > ■1111 11 ■1 > 11 > । m/z 40.10 16.72% m/z-> 0 5 10 15 20 25 30 35 40 45 50 55 60 65 Abundance #3862: Hydrogen azide 43

5000 15 28 3.20 3.40 3.60 3.80

o1 r ir 1' ■ i ■' — 11 ■11 ■ i ■111111111111 • 111 I ■' 1 ■ i' n/z-> 0 5 10 15 20 25 30 35 40 45 50 55 60 65 Abundance #109242: Isobutane 43

5000 27 39 15 50 53 57 01 1 2....... ............ .. TTTT 1 i ' ' 1 ■ I 1 1 1 1 I 1 1 1 1 I 1 1 1 1 i rr m/z-> 0 5 10 15 20 25 30 35 40 45 50 55 60 65 Abundance #109241: Isobutane 43

5000 27 39 0 1 1' i ■ ■ ■' i'' ■ ■ i' 12 15 36 TI++ ,.... 51 54 57 ......... 11 ■ ■ ■ ‘ 1 1'1111111 I'11 11r-r n/z—> 0 5 10 15 20 25 30 35 40 45 50 55 60 65

NYC-WTC_000047341