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GCMS analysis results for sample AE06408, May 2002

Machine-extracted title · confidence 100%

Laboratory report documenting GCMS analysis of sample AE06408 conducted on May 3, 2002.

NYC-WTC_000060283–000060294

Folder label: “GCMS X 3/18/02 A 4/8/02

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Scanned page image, NYC-WTC_000060290
OCR text

OCR status: ok · source: pdftotext

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\MSDCHEM\l\DATA\020409\6408.D Vial: 12 Acq On : 10 Apr 2002 1:24 am Operator: McLean Sample : 3/18 Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e

Quant Method : C: \MSDCHEM\1. . .\SCANAPR0902 .'M (Chemstation Integrator) Title : Method 508 GC/MS Scan Library : C:\DATABASE\nist98.1 ★******************************************************************** Peak Number 2 Hydrogen azide Concentration Rank 3

R.T. EstConc Area Relative to ISTD R.T. 3.43 0.28 ug/1 212092 1,4-Dichlorobenzene-d4 10.67

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Hydrogen azide 43 HN3 007782-79-8 1 2 Mercaptamine 77 C2H7NS 000060-23-1 1 3 l-Tetrazol-2-ylethanone 112 C3H4N4O 1000195-06-4 1 4 Isobutane 58 C4H10 000075-28-5 1 Abundance Scan 59 (3.426 min): 6408.D (-51) (-) m/z 43.10 100.00% 4)3

5000 I, 320 3.40 3.60 3.80 51.................................................................................. I ‘ ‘ I ' ' ' ' I ' ' ' ' I ' ' ' ' I ' m/z 48700 19.55% Ti/z-> 10 20 30 40 50 60 70 80 90 100 110 120 Abundance #3862: Hydrogen azide 43

253 15 .,11 , ■ , 320 3.40 3.60 3 80 28 m/z 4^700 2.35%

mZz-> LJUJV 10 20 30 40 ■ 'so 60 70 'sb' " 'do' " ioo' ‘ i-io “ 120 Abundance #664: Mercaptamine 33

320 3.40 3.60 3.80 5000 “m/z 51.00 1.43%

18 59 70 77 mfe-> 10 20 30 40 50 60 70 80 90 100 110 120 Abundance #4641:1-Telrazol-2-ylethanone 40 3.20 3.40 3.60 3.80

553 28

nfe-> ... 10 20 7 30 ., 40,1 50 55 60 69 70 80 84 90 100 110 113 120

6408.D SC7kNAPR0902 .M Thu May 02 14:13:01 2002 Page 4

NYC-WTC_000060290

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NYC-WTC_000060290Source: NYC Law Department, mirrored locally

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