GCMS analysis results for sample AE06408, May 2002

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Library Search Compound Report

Data File : C:\MSDCHEM\l\DATA\020409\6408.D Vial: 12 Acq On : 10 Apr 2002 1:24 am Operator: McLean Sample : 3/18 Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e Quant Method : C:\MSDCHEM\1...\SCANAPR0902.M (Chemstation Integrator) Title : Method 508 GC/MS Scan Library : C:\DATABASE\nist98.1 ********************************************************************* Peak Number 1 Acetonitrile, dichloro- Concentration Rank 2 ■

R.T. EstConc Area Relative to ISTD R.T. 3.32 0.47 ug/1 362168 1,4-Dichlorobenzene-d4 10.67

Hit# of 5 . Tentative ID MW MolForm CAS# Qual

1 Acetonitrile, dichloro- 109 C2HC12N 003018-12-0 83 2 Acetonitrile, dichloro- 109 C2HC12N 003018-12-0 64 3 Thiirane, methyl- 74 C3H6S 001072-43-1 4 4 Allyl mercaptan 74 C3H6S- 000870-23-5 4 Abundance Scan 41 (3.320 min): 6408. D (-33) (-) m/z 74.00 100.00% 7l4

5000 82

38 47 r ■iVz-> 10 20 30 -uX 40 50 ' ' I ' ' ' ' I ' . 60 70 80 ' ' I ' ' ' ' I ' ' ' ' i ' ' ' ' I 90 100 110 3.20 3.30 3.40 3.50 3.60 3.70 m/z 82.00 46.50% Abundance #28338: Acetonitrile, dichloro- 7#

5000 82 3.20 3.30 3.40 3.50 3.60 3.70 47 m/z 76.00 28.89% 35 12 62 ' I ' ' ' ' I ‘ ' I I................... Ti/z-> 10 20 30 40 6050 70 80 90 100 110 Abundance #115342: Acetonitrile, dichloro- TH 35 I ’' '' P '' *7 3.20 3.30 3.40 3.50 3.60 3.70 5000 82 m/z^ 84.00 28.10% 47

■nZz-> 10 20 30 4p__5q__^__70__80__9p__l0q__110 Abundance #115343: Thiirane, methyl­ al 7l4 3.20 3.30 3.40 3.50 3.60 3.70 m/z 47.05 22.80% 553

47 I , [I, ■ 6^ ,J m/z-> 10 20 30 40I 50 60 70 80 90 100 110 3.20 3.30 3.40 3.50 3.60 3.70

6408.D SCANAPR0902.M Thu May 02 14:12:59 2002 Page 3

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