GC/MS analysis report for sample AE06410, May 3 2002

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Library Search Compound Report

Data File : C:\MSDCHEM\l\DATA\020409\64T0.D Vial: 14 Acq On : 10 Apr 2002 3:16 am Operator: McLean Sample : 3/18 Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e Quant Method : C:\MSDCHEM\1...\SCANAPR0902.M (Chemstation Integrator) Title : Method 508 GC/MS Scan Library : C:\DATABASE\nist98.1 ********************************************************************* Peak Number 2 Acetic acid, 3-[1,3]dioxola... Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T.

5.55 1.32 ug/1 1014130 1,4-Dichlorobenzene-d4 10.67

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Acetic acid, 3-[1,3]dioxolan-2-y... 174 C8H14O4 1000186-02-3 45 2 3-Pentanol, 3-methyl- 102 C6H14O 000077-74-7 9 3 N-Ethyl formamide 73 C3H7NO 000627-45-2 5 4 1-Butanamine, 2-methyl-_______________ 87 C5H13N 000096-15-1 5 Abundance Scan 421 (5.553 min): 6410.D (-417) (-) in/z 73710 100.00% 7|3

5000 43

520 5.40 5.60 5.80 55 87 m/z 43.10 32.05% mfe-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 Abundance #25344: Acetic acid, 3-[1,3]dioxolan-2-ylpropyl ester 70

5000 520 5.40 5.60 5.80 43 m/z 41.10 13.02% 27 55____ 87 113 131 174 I ’' ''I'l........'I’l'i''' I " " I ■ " 'I nfe-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 Abundance #114875: 3-Penfanol, 3-methyl- 7|3

5 20 5.40 5.60 5.80 5000 Wz 45710 11.30% 55 27 87 15 i.i, 37ill , 63 I ... I' ‘'' I ‘ ‘' 1“ ‘' p-rTTpr-TTry n/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 Abundance #857: N-Ethytformamide 33 T 520 5.40 5.60 5.80 73 m/z 71.10 6.17% 5000 44 58

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n/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 520 5^0 5.60 5.80

6410.D SCANAPR0902.M Thu May 02 14:15:35 2002 Page 4

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