GC/MS analysis report for sample AE06410, May 3 2002

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Data File C:\MSDCHEM\l\DATA\020409\6410.D vial: 14 Acq On 10 Apr 2002 3:16 am Operator: McLean Sample 3/18 Inst : Instrumen Mise : Multiplr: 1.00 MS Integration Params: LSCINT.e

Quant Method : C:\MSDCHEM\1.,;\SCANAPR0902.M (Chemstation Integrator) Title : Method 508 GC/MS Scan Library : C:\DATABASE\nist98.1 ********************************************************************* Peak Number 3 Anthracene-dlO- Concentration Rank 3 R.T. EstConc Area Relative to ISTD R.T. 31.14 0.22 ug/1 268163 Phenanthrene-dl0 30.92 Hit# of 5 Tentative ID MW MolForm CAS# Qua! 1 Anthracene-dlO- 188 C14D10 001719-06-8 86 2 Phenanthrene-dlO 188 C14D10 001517-22-2 72 3 3-Amino-4-methyl-6-methoxyquinoline 188 C11H12N2O 1000213-71-3 64 4 6-Hydroxy-2-phenyl-3(2H)-pyridaz... 188 C10H8N2O2 1000224-53-6 39 Abundance Scan 4775 (31.135 min): 6410.D (-4766) (-) m/z 188.10 100.00% 1(8

23

80 94 30.80 31.00 31.20 31.40 ... ....... . . .............. I m/z 184.10 14.79% n/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #79826: Anthracene-dlO- 1(8

5000 1 y.80 31.00 31.20 31.40 m/z .94.10 14.19% RR 160 I

Tife-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance ■ #79827: Phenanthrene-dlO 1^8 I _ y.8O 3100 31.20 31.40 5000 m/z 189.10 14.06%

RR 94 160

Ti/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #79771:3-Amino-4-melhyl-6-methoxyquinoline 1(8 -XX— 30.80 31.00 31.20 31.40 m/z ,80.10 13.62% 145 5000

41 51 63 77 89 iq2 130 \ ■..........................................................................

•Tj-m- rFp-mj Tife-> 10 20 30 40 50 60 70 80 90 100110 120 130 140 150 160 170 180 190 30,80 31.00 31,20 31.40

6410.D SCANAPR0902.M Thu May 02 14:15:37 2002 Page 5

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