GCMS analysis results for sample AE06304, April 2002

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Library Search Compound Report Data File C:\MSDCHEM\1\DATA\020408\6304.D Vial: 12 Acq On 8 Apr 2002 9:07 pm Operator: McLean Sample 3/18 Inst : Instrumen Mise : Multiplr: 1.00 MS Integration Params: LSCINT.e Quant Method : C:\MSDCHEM\1... \SCANAPR0902 .M (Chemstation Integrator) Title : Method 508 GC/MS Scan Library : C:\DATABASE\nist98.1 Peak Number 3 Anthracene-dlO- Concentration Rank 3

R.T. EstConc Area Relative to ISTD R.T.

31.14 0.10 ug/1 319029 Phenanthrene-dl0 30.93

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Anthracene-dlO- 188 C14D10 001719-06-8 86 2 Phenanthrene-diO 188 C14D10 001517-22-2 78 3 3-Amino-4-methyl-6-methoxyquinoline 188 C11H12N2O 1000213-71-3 45 4 Naphthalene, 1,7-dimethoxy- 188 C12H1202 005309-18-2 45 Abundance Scan 4775 (31.135 min): 6304.D (-4765) (-) m/z 188.10 100.00% 188

5000

80 94 30.80 31.00 31.20 31,40 160 O TT n p-m ITT rp-n TTTTTT my TH -r-, । ,. , . । > nr. । > mmTT T m/z 94.10 16.64% n/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160170 180 190 Abundance #79826: Anthracene-d10- 188

5000 30.80 31.00 31.20 31.40 m/ z 189.10 14.41% 17 30 42 52 68 66 80 94 160 , . 108118 132 0 S J-TT T rj r r 1» 11 I 1111 I I 11 H T IT TITT T ) 1 It TTIU—ng—dTT‘146.4+4,179179—. TT mz-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #79827: Phenanthrene-d1 0 188

30 80 31.00 31.20 31.40 5000 m/ z 184.10 14.16%

80 94 160 30 42 52 66 mlz-> 11 108118 132 0 TDWTTTTTTTTTTTTHTTTH TTTTT 10 20 30 40 50 60 70 80 90 100 110120 130 140 150 160 170 180 190 146—4.170179— TT

Abundance #79771:3-Amino-4-methyl-6-methoxyquinoline ------- 188 30.80 31.00 31.20 31.40 m/z 80.10 13.17% 145 5000

117 41 51 63 77 89 102 130 O-p 159 - 173 I 1 1 1 i ' ■ I ’ * i ' 1 * 4 I 1 * ' 1 1 m/z—> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 30.80 31.00 31.20 31.40

63 04.D SCANAPR0902 .M Tue Apr 09 15:15:00 2002 Page 5

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