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GCMS analysis results for sample AE06305, April 2002

Machine-extracted title · confidence 100%

Laboratory report documenting GCMS analysis of sample AE06305 conducted on April 17, 2002.

NYC-WTC_000039353–000039362

Folder label: “GCMS X 3/18/02 A 4/8/02”

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NYC 9/11 Public Portal Document

Library Search Compound Report Data File C:\MSDCHEM\l\DATA\020408\6305.D Vial: 13 Acq On 8 Apr 2002 10:02 pm Operator: McLean Sample 3/18 Inst Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e

Quant Method : C:\MSDCHEM\1... \SCANAPR0902.M (Chemstation Integrator) Title : Method 508 GC/MS Scan Library : C:\DATABASE\nist98.1 Peak Number 2 Anthracene-dlO- Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T. 31.14 0.11 ug/1 393655 Phenanthrene-dl0 30.93 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Anthracene-dlO- 001719-06-8 87 188 C14D10 2 Phenanthrene-diO 001517-22-2 72 188 C14D10 3 Naphthalene, 1,7-dimethoxy- 005309-18-2 45 188 C12H1202 4 2-Quinolinecarboxaldehyde, 8-hyd... 188 C10H8N2O2 005603-22-5 45 Abundance Scan 4776 (31.141 min): 6305.D (-4766) (-) m/z 188.10 100.00% US

5000

80 94 40 158 30.80 31.00 31.20 31.40 O m ' i ■ " 1 r 1 " 111 " i " " i IT miz->10 20 30 40 50 60 70 80 SO 100110 120 130 140 150 160 170 180 190 mmPPTT i’’ m/Z 189.10 16.44%

Abundance #79826: Anthracene-d 10- 1tS

—.................................... 5000 30.80 31.00 31.20 31.40 m/ z 94.20 16.15% 80 94 160 179179all—. 17 30 42 52 66 108 118 132 146 ,|| 0 TTWTITTTTTTT 1H...... 1 1——] T TTTTTTTTTT m/z-> 10 20 30 40 50 60 70 80 90 100110 120 130 140 150 160 170 180 190 Abundance #79827: Phenanthrene-d10 1tS ' ' i ■ ■ ' ' i ■ ■ TT | . . . . ] 1 > 1 I ( I 30.80 31.00 31.20 31.40 5000 m/Z 184.10 15.38%

80 94 160

m/z-> 0 30 42 52 66 1464 170179 । । 11 i । i | । । 11 11 । 11 ] H 11; 11 I 1111 H fi r 11 11— 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 108 118 nu T T] 132

Abundance #79804: Naphthalene, 1,7-dimethoxy- 173 188 30.80 31.00 31.20 31.40 m/z ,80.10 12.83% 5000 102 115 145 130

m/z—> 0 ______ 51 63 75 .. I _ ________________ ‘ I *'" 1111 ‘ I* ‘'111 H1111" 11''' I" 1111111111'11 H 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 158 TTTTT TTTTT ........................... 30.80 31.00 31.20 31.40

6305.D SCANAPR0902.M Tue Apr 09 15:15:44 2002 Page 4

NYC-WTC_000039361

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NYC-WTC_000039361Source: NYC Law Department, mirrored locally

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