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GCMS analysis results, sample AE09771, May 2002

Machine-extracted title · confidence 100%

Laboratory report for sample AE09771 showing surrogate recovery and unknown compounds from May 9, 2002.

NYC-WTC_000043893–000043918

Folder label: “GCMS X 4/25/02 A 5/7/02

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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File C:\MSDCHEM\1\DATA\050602\9771.D Vial: 24 Acq On 7 May 2002 6:25 am Operator: Mclean Sample 4/25 Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e

Quant Method : C:\MSDCHEM\1\METHODS\050102.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L

Peak Number 14 Anthracene-dlO- Concentration Rank 5

R.T. EstConc Area Relative to ISTD R.T.

23.11 0.47 ug/L 393480 Phenanthranene-dl0 22.95

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Anthracene-diO- 188 C14D10 001719-06-8 90 2 Phenanthrene-dlO 188 C14D10 001517-22-2 78 3 2-Quinolinecarboxaldehyde, 8-hyd... 188 C10H8N2O2 005603-22-5 40 4 Naphthalene, 1,7-dimethoxy- 188 C12H1202 005309-18-2 36 Abundance Scan 3409 (23.109 min): 9771 .D (-3403) (-) m/z 188.10 100.00% us

5000

------- 43 52 66 80 *4 T111111111110001010100201011171000—mu00uuu 160 4 22.80 23.00 23.20 23.40 m/ z 94.10 12.83%I m/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 ft Abundance #79826: Anthracene-d10- 188

5000 11 i 1 1 1 1 T 1 ' I 1 1 1 1 I 1 1 1 1 I 22.80 23.00 23.20 23.40 m/z 160.10 12.67% SA 80 94 160 1 ft m/z—> 17 30 42 52 j I | I I u | | | I r[ i I i I | I I I | | I I I r । I I I i । i i I I

10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 , I rr t | | TuuaTHt 108 118 132 146—+41791794—— Abundance #79827: Phenanthrene-d10 US ........................................ , 22.80 23.00 23.20 23.40 5000 m/z 92.10 11.76%|

80 94 160 30 42 52 66 , m/z-> +108.118,132 146—4179179 l. ■ -j-rr-rr-j-t , , ■ । 1 I i , । , I t , | i . I l | I

10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #125696: 2-Quinolinecarboxaldehyde, 8-hydroxy-, oxime 1 1 1 1 1 ' ‘ T 1 11 | I 1 I I | 1 M I | US 22.80 23.00 23.20 23.40 m/z 189.10 11.76%| A 5000

143 89 115 TITTTT]PTTTIWTTTTTTTT TTT 5.1 64 ironir 1 158 170 4 76 I 102 |i 130 11 ■ 11111 < 1111111 ■ • । ■ i ■ ■ r । । > । । i । > । । mfa-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 22.80 23.00 23.20 23.40

9771.D 050102.M Tue May 07 15:44:23 2002 Page 17

NYC-WTC_000043914

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NYC-WTC_000043914Source: NYC Law Department, mirrored locally

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