GCMS analysis results for sample AE06304, April 2002

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Library Search Compound Report

Data File C:\MSDCHEM\1\DATA\020408\6304.D Vial: 12 Acq On 8 Apr 2002 9:07 pm Operator: McLean Sample 3/18 Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e Quant Method : C:\MSDCHEM\1... \SCANAPR0902.M (Chemstation Integrator) Title : Method 508 GC/MS Scan Library : C:\DATABASE\nist98.1 Peak Number 2 Formamide, N-(cyanomethyl)- Concentration Rank 2 R.T. EstConc Area Relative to ISTD R.T. 3.41 0.13 ug/1 254831 1,4-Dichlorobenzene-d4 10.67 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Formamide, N-(cyanomethyl)- 84 C3H4N2O 005018-27-9 2 2 l-Penten-3-one 84 C5H80 001629-58-9 1 3 Ethanethiol, 2-amino-, hydrochlo... 113 C2H8C1NS 000156-57-0 1 4 l-Propyne, 3-chloro- 74 C3H3C1 000624-65-7 1 Abundance Scan 57 (3.414 min): 6304.D (-54) (-) m/z 40.10 100.00% 40

84 5000

47 ' i 1 ‘ 1 ■ i ■ ' 1 ■ I 1 1 1 1 i 1 1 51 3.20 3.40 3.60 3.80 Of ‘I1I —mTmPmmmPTTTTT m/z 84.00 57.24% 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 ./*MMwnll r 1 " i1 " ' i' " 11" ‘11" " 111 i ""i m/z-> Abundance #541: Formamide, N-(cyanomethyl)- 29 84 55 5000 3.20 3.40 3.60 3.80 40 m/z 47.00 15.54% 43 .36 .......... ... 0 " I'''111' " I " " I " '' I " +t ....... 1 miz-> 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 Abundance #63: 1-Penten-3-one 27 55 3.20 3.40 3.60 3.80 5000 m/z 51.05 6.54%

0 I 30 3942 Im... ........ . 1 tr i11111111' । 52 84 4"yMLAmynod.L m/z-> Abundance 5 10I—15..... 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 I [ 11 it"

#715: Ethanethiol, 2-amino-, hydrochloride —. ! . . . . J l ■ | i 1 i i ! i 1 3b 3.20 3.40 3.60 3.80 36 m/z 49.10 2.22%

5000

27 4245 59 77 33 . ............ 62 m/z-> 0 ... . v TTTTTT —H ... 1111'1111 ■ 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 —70731 3.20 3.40 3.60 3.80

6304.D SCANAPR0902.M Tue Apr 09 15:14:59 2002 Page 4

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