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GCMS analysis results, sample AE09973, May 2002

Machine-extracted title · confidence 100%

Laboratory report for sample AE09973 showing surrogate recovery and unknown compounds from May 9, 2002.

NYC-WTC_000044025–000044054

Folder label: “GCMS X 4/25/02 A 5/7/02”

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NYC 9/11 Public Portal Document

Library Search Compound Report Data File C:\MSDCHEM\1\DATA\050602\9973.D Vial : 21 Acq On 7 May 2002 3:59 am Operator: Mclean Sample 4/25 Inst : Instrumen Mise : Multiplr: 1.00 MS Integration Params: LSCINT.e

Quant Method : C:\MSDCHEM\1\METHODS\050102.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L ********************************************************************* Peak Number 7 Formamide, N-(cyanomethyl)- Concentration Rank 6

R.T. EstConc Area Relative to ISTD R.T.

4.34 0.39 ug/L 277339 1,4-Dichlorobenzene-d4 9.94

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Formamide, N-(cyanomethyl)- 84 C3H4N20 005018-27-9 7 2 1,3,5-Cycloheptatriene 92 C7H8 000544-25-2 4 3 1,3,5-Cycloheptatriene 92 C7H8 000544-25-2 4 4 1,3,5-Cycloheptatriene 92 C7H8 000544-25-2 3 Abundance Scan 214 (4.337 min): 9973.D (-208) (-) m/ z 91.10 100.00% 91

5000 84 ............ । ! ] 11I i | । r i A F] C i r-] i r 'i—i—° 40 50 65 4.00 4.20 4.40 4.60 । ’ 1 1 ' । 1 1 । 1 1 ‘ 1 । । । I , | i 58 | ' 1 i 1 1 1 1 i ' 1 1 1 i ‘ Tl | 1 । । | FT m/ z 92.10 62.71% m/z-> 0 10 20 30 40 50 60 70 80 90 100 110 Abundance #541: Formamide, N-(cyanomethyl)- 29

84 55 5000 4.00 4.20 4.40 4.60______ 40 m/z 84.00 32.78%

m/z-> I ' 1 ‘ 1 I ' 1 1 ' I ' 0 10 20 ---—4 30 40 50 61 1 i'1 ' ' 1 । 1 1 1 ' । ■ 60 70 80 I I

90 | I I I C

100 I l I

110 | FT MMMpM4ny,Alnkoic Abundance #37276: 1,3,5-Cycloheptatriene 91 I I I I I I I [ I I ) I [ I I I I I 1 I I—I—|— 4.00 4.20 4.40 4.60 5000 m/ z 50.00 16.07% 39 65 V 2 15 77 51 —45-+1457—1471-77—85.4 I 106 4 I 1 1 ' 1 I ' 11 1 I ' ' 1 1 I ' ' 1 i 1 1 ' 1 i 1 1 m/z-> 0 10 20 30 40 50 60 70 80 90 100 110 Abundance #117298: 1,3,5-Cycloheptatriene 1 1 r ‘ 1 1 i ' 1 1 । f 1 91 4.00 4.20 4.40 4.60 m/ z 83.00 12.39% 5000

65 28 39 . I 1 ' ' ' I ■ 45‘I i |511 ■ । ' ' |1111 - I । l'lI । I i i ■ I' [■,-r t ,1 . 77 85 , ■ । 1 1 ''' । ' ■ । ' I 1 1 i ' ’ ■ 1 i 1 1 m/z—> 0 10 20 30 40 50 60 70 80 90 100 110 4.00 4.20 4.40 4.60

9973.D 050102.M Tue May 07 15:51:56 2002 Page 11

NYC-WTC_000044040

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NYC-WTC_000044040Source: NYC Law Department, mirrored locally

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GCMS analysis results, sample AE09968, May 2002 · Box DEP Box 25

NYC-WTC_000043938

Gas chromatography-mass spectrometry analysis report for sample AE09968, detecting unknown compounds and 2,4-DDD surrogate with 78% recovery, dated May 9, 2002.

1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.996

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