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← Document results/DEP Box 25/GCMS X 4/25/02 A 5/7/02
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GCMS analysis results, sample AE09973, May 2002

Machine-extracted title · confidence 100%

Laboratory report for sample AE09973 showing surrogate recovery and unknown compounds from May 9, 2002.

NYC-WTC_000044025–000044054

Folder label: “GCMS X 4/25/02 A 5/7/02”

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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File C:\MSDCHEM\1\DATA\050602\9973 .D Vial : 21 Acq On 7 May 2002 3:59 am Operator: Mclean Sample 4/25 Inst : Instrumen Mise : Multiplr: 1.00 MS Integration Params: LSCINT.e Quant Method : C:\MSDCHEM\1\METHODS\050102.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L

Peak Number 6 2-Chloroethanol Concentration Rank 18

R.T. EstConc Area Relative to ISTD R.T.

4.26 0.23 ug/L 162692 1,4-Dichlorobenzene-d4 9.94

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 2-Chloroethanol 80 C2H5C10 000107-07-3 4 2 2-Chloroethanol 80 C2H5C10 000107-07-3 3 5-Hexen-3-one 98 C6H10O 024253-30-3 3 4 l-Penten-3-one 84 C5H8O 001629-58-9 3 Abundance Scan 201 (4.260 min): 9973.D (-196) (-) m/z 40.10 100.00% 40

5000 84 100 I l t ' I 1 L1 ■ I I I I I I I > I I I I I I 49 4.00 4.20 4.40 4.60 35 I I । ■ ■ ■ I | • m/z 100.10 42.29% i ' 1 1 ' i ■ ■ 1 ■ i 1 ■ ' TTl n/z-> 10 20 30 40 50 60 70 80 90 100 Abundance #1032: 2-Chloroethanol 31

5000 ' 1 1 1 h ‘ ‘‘ 4.00 4.20 4.40 4.60 m/z 84.00 39.19%

n/z~> —T++ 10 15 +24 20 30 36 43 49 40 50 61 60 70 80 80 90 100 "PWyMyMub"yyAhAnnzal, Abundance #108328: 2-Chloroethanol 31 1 1 1 1 I 1 1 1 1 I 1 ' 1 1 1 1 ' ' ' 1 1 ' 1 4.00 4.20 4.40 4.60 5000 m/z 98.10 31.30% 44

49 ............... . 1 57 63 80 1 1 1 1 1 1 1 I 1 1 1 1 i ' ■ 1 1 i 1 1 1 11 ■ ■ ■ ■ ■ r । ■. .. ।। ....... . । । । । । । । , । । /z-> 10 20 30 40 50 60 70 80 90 100 Abundance #481:5-Hexen-3-one i I i । | 7 i i I । i i i i । i i < i |l ■ ■ 29 57 4.00 4.20 4.40 4.60 m/z 43.10 29.98%

5000 41 ".Ma/Mutouowse 69 98 i ■ ' ■ ■ । 1II‘* 'I 1 ' ' ' i ' +TT ■ I ' 1 1 ■ i ' 1 ■ i ■ ■ • i t ■ ■ ■ ■ i 1 ■ । 1 1 ' ■ । 1 ■ 1 1 । 1 1 ' ' i 1 1 /z-> 10 20 30 40 50 60 70 80 90 100 4.00 4.20 4.40 4.60

9973.D 050102.M Tue May 07 15:51:54 2002 Page 10

NYC-WTC_000044039

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NYC-WTC_000044039Source: NYC Law Department, mirrored locally

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GCMS analysis results, sample AE09968, May 2002 · Box DEP Box 25

NYC-WTC_000043938

Gas chromatography-mass spectrometry analysis report for sample AE09968, detecting unknown compounds and 2,4-DDD surrogate with 78% recovery, dated May 9, 2002.

1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.996

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