GCMS analysis results, sample AE12533, June 2002

NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\MSDCHEM\l\DATA\052902\12533.D Vial: 24 Acq On : 30 May 2002 4:49 am Operator: McLean Sample : gc/ms scan 5/28 Inst : Instrumen Mise : Multiplr: 1.00 MS Integration Params: LSCINT.e Quant Method : C:\MSDCHEM\1\METHODS\052202.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L ■it * * * * * * * * it * * -it * * * * * * * * * * * * * * * * k * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * it * * * * * *

Peak Number 6 Formamide, N-(cyanomethyl)- Concentration Rank 5 R.T. EstConc Area Relative to ISTD R.T.

3.85 0.83 ug/L 651852 1,4-Dichlorobenzene-d4 9.90

Hit# of 5 Tentative ID MW MolForm CAS# Qual l Formamide, N-(cyanomethyl)- 84 C3H4N2O 005018-27-9 5/ 2 4H-1,2,4-Triazol-4-amine 84 C2H4N4 000584-13-4 5 3 Thiophene 84 C4H4S 000110-02-1 4 4 Krypton 84 Kr 007439-90-9 3 Abundance Scan 131 (3.849 min): 12533.D (-129) (-) m/z 84.00 100.00% 84

5000 47 51

38 43 '' 3.60 3,80 4.00 4.20 ' O+ - HIpmmmmmp ■ ■ i ■ ■'11 ■ m/z 86.00 50.51% z-> 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 Abundance #541: Formamide, N-(cyanomethy!)- 29

84 55 5000 3.60 3.80 4.00 4.20 40 m/z 47.00 42.96%

miz-> Of TI

Abundance i ■ ■ “ r“ ‘ ■ i Hr 36 43 -HHHH 5861 66 1 11Pmmmgt 10 15 20253035434550 55 6065 70 75 80859095

23 #107976:4H-1,2,4-Triazol-4-amine —./MMMu* „/ 84 3.60 3.80 4.00 4.20 5000 m/z 51.10 34.25?

18 42 51 36 39. , — 69 0 ......... ....... -ftr 9445— — 1 miz-> 10 15 2025303540455055 60 65 70 75 80859395 Abundance #116584: Thiophene 84 3.60 3.80 4.00 4.20 58 m/z 38.20 10.89% 45 5000 39

0 PmTTNTT 42 50 26 32 36 + +HH Hmp 1 “ “ 14 81, 6972 —H+ 7 n/z—> 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 3.60 3.80 4.00 4.20

12533.D 052202.M Mon Jun 03 11:45:29 2002 Page 9

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