Laboratory report showing GCMS analysis results for sample AE12326 including surrogate recovery data on June 10, 2002.
NYC-WTC_000014384–000014405Folder label: “GCMS X 5/28/02 A 5/29/02”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document Library Search Compound Report Data File : C:\MSDCHEM\l\DATA\052902\12326.D vial: 17 Acq On : 29 May 2002 11:07 pm Operator: McLean Sample : gc/ms scan 5/28 Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e
Quant Method : C:\MSDCHEM\1\METHODS\052202.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C: \DATABASE\NIST98 . L ********************************************************************* Peak Number 5 4H-1,2,4-Triazol-4-amine Concentration Rank 3 R.T. EstConc Area Relative to ISTD R.T. 3.96 1.74 ug/L 1112280 1,4-Dichlorobenzene-d4 9.90 Hit# of 5 Tentative ID MW MolForm CAS# Qual
1 4H-1,2,4-Triazol-4-amine 84 C2H4N4 000584-13-4 9 2 2-Butenal, 2-methyl- 84 C5H80 001115-11-3 9 3 Thiophene 84 C4H4S 000110-02-1 7 4 Thiophene 84 C4H4S 000110-02-1 7 Abundance Scan 150 (3.960 min): 12326.D (-149) (-) m/z 84.00 /100.00% 84
5000
88 37 42 47 51 360 3.80 4.00 4.20 4.40 ' ‘ I ‘“ I “ ' 111' “ I “■> 111 > 111111 j 11. ■ f 1JI 11 ■ I I! |11 r I.. 11 > > > I > ■ r. 11 ri > |. ri 11 n > 01 ' I" " 11' m/z 87.90 17.50% niz-> 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 Abundance #33490:4H-1,2,4-Triazol-4-amine 28 84
5000 ‘ 1 i ■ ■ 3.60 3.80 4.00 4.20 4.40 m/z 37.10 8.86% 13 18 20 4043 69 57 ol -HHH +#H+— ’ I—0T01011T71711HHmm nz—> Abundance 5 10 15 20 25 30 #116563: 35 40 45 50 55 60 65 70 75 80 85 90 95 2-Butenal, 2-methyl- 55 84 • • i ■ ■ ■ ■ i ■ • ■ ■ i ■ ■ ■ • i • • ■ ■ i ■ 3.60 3.80 4.00 4.20 4.40 5000 29 m/ z 42.10 8.65% 41 26 44 51 1 69________ I OlTTT] I’T 1111 38 til [ 111v 111 ii 1, 111 I11 THDTUDT Tym-rp-r Tl/Z-> 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 Abundance #116584: Thiophene 84 3.60 3.80 4.00 4.20 4.40 58 m/z 47.05 8.44% 5000 39 45 Myu 26f,>111 32!i]llI 36 ++42 11150 6972 811 mfe-> 0 .. ।....,., i > (1111111 n 11 5 111H111 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 HH 7 3.60 3.80 4.00 4.20 4.40
12326.D 052202.M Mon Jun 03 11:32:48 2002 Page 8
NYC-WTC_000014396
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NYC-WTC_000014509
Laboratory report showing GCMS analysis results for sample AE12531 including surrogate recovery data on June 10, 2002.
1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000014433
Laboratory report showing GCMS analysis results for sample AE12477 including surrogate recovery data on June 10, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000014485
Laboratory report showing GCMS analysis results for sample AE12479 including surrogate recovery data on June 10, 2002.
1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000014406
Laboratory report showing GCMS analysis results for sample AE12476 including surrogate recovery data on June 10, 2002.
1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000014532
Gas chromatography-mass spectrometry analysis of sample AE12532 performed on 6/10/02, detecting 2,4-DDD surrogate at 77% recovery.
1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000014460
Laboratory report showing GCMS analysis results for sample AE12478 including surrogate recovery data on June 10, 2002.
1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000014552
Laboratory report showing GCMS analysis results for sample AE12533 including surrogate recovery data on June 10, 2002.
1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000012966
Laboratory report presenting analytical results for target compounds and surrogate recovery data for water sample AE11906.
1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000013454
Laboratory report documenting GCMS analysis of sample AE11926 conducted on June 4, 2002, including surrogate recovery data.
1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000013476
Laboratory report documenting GCMS analysis of sample AE11926 conducted on June 4, 2002, including surrogate recovery data.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000014125
Laboratory report documenting gas chromatography-mass spectrometry analysis of environmental sample AE12475 conducted on June 4, 2002.
1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000013624
Laboratory report documenting GCMS analysis of sample AE12161 conducted on June 5, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗No available related records indexed in this group.
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NYC-WTC_000014348
DEP document containing gas chromatography-mass spectrometry data from late May 2002.
Filed in the same folder
NYC-WTC_000014349
Document page referencing GCMS methods and sample identification number NYC-WTC_000014348 dated May 28, 2002.
Filed in the same folder
NYC-WTC_000014351
Laboratory report showing GCMS blank analysis results for volatile organic compounds in sample AE12326 on June 3, 2002.
Filed in the same folder
NYC-WTC_000014375
Laboratory report showing GCMS calibration data for volatile organic compounds in sample AE12326 on June 3, 2002.
Filed in the same folder
NYC-WTC_000014379
Laboratory report showing GCMS reference analysis data for volatile organic compounds in sample AE12326 on June 4, 2002.
Filed in the same folder