GCMS analysis results for sample AE11932, June 2002

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Library Search Compound Report

Data File : C:\MSDCHEM\l\DATA\052302\11932.D Vial: 12 Acq On : 23 May 2002 6:56 pm Operator: Mclean Sample : 5/22ad Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e Quant Method : C:\MSDCHEM\1\METHODS\052202.M (Chemstation Integrator). Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L ********************************************************************* Peak Number 12 4H-1,2,4-Triazol-4-amine Concentration Rank 15

R.T. EstConc Area Relative to ISTD R.T.

4.79 0.31 ug/L 215422 1,4-Dichlorobenzene-d4 9.90

Hit# Of 5 Tentative ID MW MolForm CAS# Qua

1 4H-1,2,4-Triazol-4-amine 84 C2H4N4 000584-13-4 7 2 Thiophene 84 C4H4S 000110-02-1 4 3 Thiophene 84 C4H4S 000110-02-1 4 4 Thiophene■ 84 C4H4S 000110-02-1 4 Abundance Scan 291 (4,789 min): 11932.D (-289) (-) "* 84.00 TOO.00% 84

5000 38 44 4.40 4.60 4.80 5.00 5.20 0- mmmmmHHu. + 50 I’’IAAIAAAA’/’I’A’’L l““l m/z 86.00 78.20% mtz~> 0 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 Abundance #33490:4H-1,2,4-Triazol-4-amine 28 84

5000 ‘ i ‘ ■ I ■ • ‘ 1 l ‘ ‘ ‘ I ‘ ‘ ' 1 I • ‘ 4.40 4.60 4.80 5.00 5.20 m/z 44.10 24.56%

niz-> Abundance 0- 0 13 18 I > ni!>11 I|I lli! ■••«11 ....... .X...................... 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 #33732: Thiophene

45 58 84 "hi” 4.40 4.60 4.80 5.00 5.20 5000 m/z 38.00 21.68% 39

1 26 32 50 । 69

niz-> 0- 12 TTppnp—pHt— iii1111 ■ 1111 ■I"1 'ih" 0 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 .. 94488 77 Abundance #116584: Thiophene 84 4.40 411—— 4.60 4.80 ll 5.00 5.20 58 m/ z 36.10 13.78% 45 5000- 39 26 32 50 69 ---------- H 11111111111 I |i i n 11 n l| 11111! i i9^l l lmn T-p-f mfc-> 0 o 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 4.40 4.60 4.80 5.00 5.20

11932.D 052202.M Wed May 29 09:51:37 2002 Page 15

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