GCMS analysis results, sample AE12533, June 2002

NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\MSDCHEM\1\DATA\052902\12533.D Vial: 24 Acq On : 30 May 2002 4:49 am Operator: McLean Sample : gc/ms scan 5/28 Inst : Instrumen Mise : Multiplr: 1.00 MS Integration Params: LSCINT.e Quant Method : C:\MSDCHEM\1\METHODS\052202.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L ********************************************************************* Peak Number 5 Ethanol, 2,2-dichloro- Concentration Rank 9 R.T. EstConc Area Relative to ISTD R.T. 3.81 0.68 ug/L 538727 1,4-Di chlorobenzene -d4 9.90

Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Ethanol, 2,2-dichloro- 114 C2H4C120 000598-38-9 2/ 2 Ethyl Chloride 64 C2H5C1 000075-00-3 1 3 2-Chloroethanol 80 C2H5C10 000107-07-3 1 4 1-Propanol, 3-chloro- 94 C3H7C1O 000627-39-5 1 Abundance Scan 125 (3.814 min): 12533.D (-123) (-) m/z 49.10 Z00.00% 40

5000 43 35 82 3.40 3.60 3.80 4.00 4.20 01 • ' I ‘ ‘ ‘ I ‘ ‘ ' I ‘ ' I ‘ ‘ m/z 51.10 38.41% miz-> 10 20 30 40 50 60 70 80 90 100 110 120 Abundance #1082: Ethanol, 2,2-dichloro- 31

5000 | ‘ * l * * * i I * * * * ! * ‘ * » J * * 3.40 3.60 3.80 4.00 4.20 m/z 43.10 31.71% 25 , 37 43 49 55 61 70 Tl, 83 01 ■ 1 l “ ■ 11 ' 1 P"t’’t1111—**— 96 103 114 niz-> 10 20 30I 40 50 60 70 80 90 100 110 120 Abundance #107943: Ethyl Chloride 23 A” 3.40 3.60 3.80 4.00 4.20 64 5000 m/z 81.90 23.32% 49 15 35

niz->10 0: - 20 -r40■ . .'Hl501- ■ ■ ■60T'1 30 ■ i ■ ■ ■ ■ i • • ■ ■ i ■ ■1 • i ■ • ■ ' i • ■ ‘ 1 i • ■ 70 80 90 100 110 120 Abundance #1032:2-Chloroethanol i ' 1 ■ ■ i ■ ' 1 31 3.40 3.60 3.80 4.00 4.20 m/ z 35.10 21.95%

5000 y M "WA 15

n/z-> 0 .... 1,47211, , 37,41.49,, 61 80 ■ ‘ I1 1 • 1 I 1 1 '‘T''11 I 111'i•'■ ■i■ 1 ' 1 1 1 ' 10 20 30 40 50 60 70 80 90 100 110 120 3.40 3.60 3.80 4.00 4.20

12533.D 052202.M Mon Jun 03 11:45:28 2002 Page 8

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