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GCMS analysis results, Sample AE08263, April 22, 2002

Machine-extracted title · confidence 100%

GCMS analysis report for sample AE08263 showing surrogate recovery and unknown compound screening on April 22, 2002.

NYC-WTC_000048333–000048354

Folder label: “GCMS X 4/9/02 A 4/17/02

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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\MSDCHEM\1\DATA\020417\08263.D Vial: 20 Acq On : 18 Apr 2002 1:07 am Operator: Nefliu Sample : sample Inst Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e Quant Method : C:\MSDCHEM\1\METHODS\041702SCAN.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L ********************************************************************* Peak Number 4 Ethanol, 2,2-dichloro- Concentration Rank 10

R.T. EstConc Area Relative to ISTD R.T.

3.80 0.28 ug/L 208183 1,4-Dichlorobenzene-d4 9.98

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Ethanol, 2,2-dichloro- 114 C2H4C12O 000598-38-9 2 2 Propanoyl chloride 92 C3H5C1O 000079-03-8 2 3 2-Chloroethanol 80 C2H5C1O 000107-07-3 2 4 2-Chloroethanol 80 C2H5C1O 000107-07-3 2 Abundance Scan 123 (3.802 min): 08263 D (-121) (-) m/z 35.10 100.00% 35

5000 51 84

41 3.40 3.60 3.80 4 00 4.20 0- I m/z51.0045.01% n/z-> 90 100 110 120 Abundance 0 10 20 30

31 40 50 60 70 80 #1082: Ethanol, 2,2-dichloro- Apo//"uhh-y/ao 5000 340 3.60 3 80 4 00 4.20 m/z 40.00 37.57% 0* 1 ioi| 21, 37 43 49 55 61 70 77 83 96 103 । । 114 i >■1 1 I 11' '-11............ . ............. ... । । । i'| i'i'i , । . , . . । . I i . । । . n/z- > 0 10 20 30I 40 50 60 70 80 90 100 110 120 Abundance #472: Propanoyl chloride 29 57 3.40 3.60 3.80 4 00 4.20 5000 m/z 83.90 33.27%

14 35 42 4g 65 71 82 91 "Mapaty"Mama n/z-> 0- 11,211170020 0 10 20 1- 30 40 50 1 1 60 । । 70 । । ■ • ■ ■ । 80 90 । ■ i ■ ■ ■ ■ । ■ ■ ■ ' । 100 110 120 '

Abundance #108328: 2-Chloroethanol

cAAuLtodnasdnak 31 3.40 3.60 3.80 4.00 4.20 m/ z 82.90 32.09%

5000 44

0 0 10 20 30 +371.4,57,63, 40 50 60 70 80 TIT 80 90 100 110 120 ■n/z-> 340 3.60 3.80 4.00 4.20

08263 .D 041702SCAN.M Thu Apr 18 09:51:13 2002 Page 9

NYC-WTC_000048345

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NYC-WTC_000048345Source: NYC Law Department, mirrored locally

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