GCMS analysis results, Sample AE08263, April 22, 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\MSDCHEM\1\DATA\020417\08263.D Vial: 20 Acq On : 18 Apr 2002 1:07 am Operator: Nefliu Sample : sample Inst Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e

Quant Method : C:\MSDCHEM\1\METHODS\041702SCAN.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L

Peak Number 5 1,2-Propadiene Concentration Rank 8

R.T. EstConc Area Relative to ISTD R.T.

3.86 0.29 ug/L 215675 1,4-Dichlorobenzene-d4 9.98

Hit# of 5 Tentative ID MW MolForm CAS# Qual

l 1,2-Propadiene 40 C3H4 000463-49-0 9 2 Imidazol, 4-fluoro- 86 C3H3FN2 030086-17-0 2 3 3-Butyn-l-ol 70 C4H60 000927-74-2 2 4 1-Propyne 40 C3H4 000074-99-7 2 Abundance Scan 132 (3.855 min) 08263.D (-131) (-) m/z 40.00 100.00% 4b

35 86 5000

43 51 48 3.60 3.80 4.00 4.20 0+ ■' i ■ ■ " r ■ ■' i" " i1''' i' "11 ‘' " i " " r " ‘ r 1" i " " i " " i" " i '' r ' ■' i' m/z 85.90 65.52% n/z-> 5 10 15 20 25 30 Abundance 35 40 45 50 55 60 65 70 75 80 85 90 95 #1401: 1,2-Propadiene 40 "Wp"MWuw 5000 37 3.60 ' 3.80 4.00 ' 4.20 m/z 35.10 62.36% 1215 20 26 2932 1 0 TTI i ■ HI|...i| ■■ ■ 111............ 1 +TTTT ‘ ‘I"E‘I0-TTEE‘ITEOII‘I‘‘ITCWTVTTITTTTTT"‘‘INT n/Z- > 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 Abundance #34862: Imidazol, 4-fluoro- 85 W 5000

59 1)1 01 • I ■ ■ " I ’ TTHPT 1 J'1 I I 11 I ' 1 I " •' 11 > > ’ I ITT Tl/Z--> 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 Abundance #108417- 3-Butyn-1-ol 40 3.60 3.80 4 00 4 20 m/ z 51.00 21.15% 31 5000 okodhtuya 27 37 •■3 50 55 69 12 15 18 0 TITUMTTHTTT ,1, , T II.... illlM. mm ................................................ n/Z-> 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 3.60 3.80 4.00 4.20

08263.D 041702SCAN.M Thu Apr 18 09:51:13 2002 Page 10

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