GCMS analysis results for sample AE08252, April 2002

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Library Search Compound Report

Data File : C:\MSDCHEM\1\DATA\020417\08252 .D Vial: 10 Acq On : 17 Apr 2002 4 :52 pm Operator: Nefliu Sample : sample Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e Quant Method : C: \MSDCHEM\1\METHODS\041702SCAN.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L

Peak Number 4 1,2-Propadiene Concentration Rank 17

R.T. EstConc Area Relative to ISTD R.T.

4.38 0.22 ug/L 227080 1,4-Dichlorobenzene-d4 9.99

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 1,2-Propadiene 40 C3H4 000463-49-0 5 2 1,3,5-Cycloheptatriene 92 C7H8 000544-25-2 4 3 1,3,5-Cycloheptatriene 92 C7H8 000544-25-2 4 4 1,6-Heptadiyne 92 C7H8 002396-63-6 3 Abundance Scan 222 (4,384 min): 08252.D (-216) (-) m/ z 91.00 100.00% 91 40 51

5000

86, 4.00 4.20 440 4 60 4.80

n/z- > 0- 0 t ' ' ' ' I ' ' ' 1 I ' ' 1 r I 10 20 30 40 L 150 60 ........... n! 70 80 90 100 110 40.00 m/z RRMRWy 76.44% Abundance #1401' 1.2-Propadiene 4b

5000 4 00 4 20 4.40 4 60 4.80 m/z 92.10 68.19%

-n/z—> 01 ..... 0 .10 20 32, 1,40 30 50 60 70 80 90 100 110 Abundance #37276 1,3,5-Cycloheptatriene 91

4.00 4 20 4.40 4 60 4.80 5000 m/z51.0067.93% 39 65 VMl/hwhipjanussu 01 2... 157 1 1 I ' 1 ' ' I ' 1 ' ' I ' ' 1 ' I ' ----- .1, 45 51 60,1.1. 71 77 86, . 106 n/z-> 0 10 20 30 40 50 60 70 80 90 • 100 110 Abundance #117298 1,3,5-Cycloheptatriene 91 4 00 4 20 4 40 4.60 4.80 m/ z 49.00 37.04% 5000 "PMuApmat 65 28 39 0 I 45 5]., 601,,,1 T1 1 771** I 1 186' ''l i ■ ■ ■ ■ i 1 ' l l ' l^l I n/z-> 0 10 20 30 40 50 60 70 80 90 100 110 4.00 4.20 4.40 4 60 4 80

08252.D 041702SCAN.M Thu Apr 18 09:13:57 2002 Page 9

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