GCMS analysis results for sample AE06409, May 2002

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Library Search Compound Report Data File : C:\MSDCHEM\1\DATA\020409\6409.D Vial: 13 Acq On : 10 Apr 2002 2:20 am Operator: McLean Sample : 3/18 Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e Quant Method : C:\MSDCHEM\1...\SCANAPR0902 .M (Chemstation Integrator) Title : Method 508 GC/MS Scan Library : C:\DATABASE\nist98.1 ********************************************************************* Peak Number 2 Acetic acid, 3-[1,3]dioxola.... Concentration Rank 1 R.T. EstConc Area Relative to ISTD R.T.

5.55 1.37 ug/1 1001580 1,4-Dichlorobenzene-d4 10.66 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Acetic acid, 3-[1,3]dioxolan-2-y... 174 C8H14O4 1000186-02-3 50 2 N-Ethylformamide 73 C3H7NO 000627-45-2 5 3 1-Butanamine, 3-methyl- 87 C5H13N 000107-85-7 5 4 1-Butanamine, 2-methyl- 87 C5H13N 000096-15-1 5 ^bundance Scan 421 (5.553 min): 6409. D (-414) (-) m/z 73.10 100.00% 7b

ciiliSlI

43

87 520__5;40_5;60__5W___ ,1 m/z 43.10 31.51% I' " ' 1" " I ■nlz-> 0 10 20 30 40 50 60 70 80 90 100110 120 130 140 150 160 170 180 Abundance #25344: Acetic acid, 3-[1,3]dioxolan-2-ylpropyl ester 7b

5000 5.20 5.40 5.60 5.80 43 in/z 41.10 11.80% 27 . I 55 TiVy 113 131 174 p"’I I " I"'' I" Ti/z-> 0 10 20 30 40 . 50 60 70 80 90 100 110 120 130 140 150 160 170 180 Abundance #857: N-Ethylformamide 3b 73 5.20 5.40 5.60 5.80 m/z 45.10 10.54% 44 58

■n/z-> "'I'' 0 JU I " '' I 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 I'' " I'' " I

Abundance #670:1-Butanamine, 3-methyl- , ...................... 33 520_540__5;6g__S8p____ m/z 71.10 7.35% 553

2 rn/z-> 0 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 5.20 5.40 5.60 5.80

6409.D SCANAPR0902.M Thu May 02 14:14:19 2002 Page 4

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