GCMS Method 508 sample analysis results, April 10 2002

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Library Search Compound Report

Data File : C:\MSDCHEM\l\DATA\020409\6407.D Vial: 11 Acq On : 10 Apr 2002 12:28 am Operator: McLean Sample : 3/18 Inst Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e Quant Method : C:\MSDCHEM\1...\SCANAPR0902. M (Chemstation Integrator) Title : Method 508 GC/MS Scan Library : C:\DATABASE\nist98.1 Peak Number 1 Acetic acid, 3-[1,3]dioxola... Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T. 5.55 1.26 ug/1 845991 1,4-Dichlorobenzene-d4 10.67 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Acetic acid, 3-[1,3]dioxolan-2-y... 174 C8H14O4 1000186-02-3 50 2 N-Ethylformamide 73 C3H7NO 000627-45-2 5 3 1-Butanamine, 3-methyl- 87 C5H13N 000107-85-7 5 4 1-Butanamine, 2-methyl- 87 C5H13N 000096-15-1 5 Abundance Scan 421 (5.553 min): 6407.D (-413) (-) m/z 73.10 100.00% 713

553 43 , I 87 _5:2g__5,40__5W 5.80 -rr-rp I"'' I T' Urp-rAy r I p " ' I" ' * I m/z 43.10 31.79% T)/Z-> 0 10 20 30 40 50 60 70 80 90 100110 120 130 140 150 160 170 180 Abundance #25344: Acetic acid, 3-11,3]dioxolan-2-ylpropyl ester 713

5000 5,2g_540__5W_^;8g^^_ Wz 41.10 11.93% .I 87 113 131 174 -rrrp p TiZz-> 0 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 “Mjundance #857: N-Ethylformamide 3) 73 5.20 5.40 5.60 5,80 553 m/z 45.10 11.52%' 44 58

18 I -m-p- ''' I'''' 1'''' t''' '"I'' " I p-rrrpTTTym-TTTTTTj Tl/Z-> 0 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 Abundance #670:1-Butanamine, 3-methyl- 33 520 5.40 5 60 5.80 m/z 71.10 7.34% 5000

2 f."', 55 70 87 ^rrTTymryTTVtYrTTT-l-rr^^ I" " I I " '' r ‘' I' " ‘ I'' " P ' ‘' I ' I ' ' ' ' i ' ' ' ’ I ' ' ' ' I ' ‘ ' I ' ■nZz-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 5205405,60 5^

6407.D SC7\NAPR0902 ,M Thu May 02 14:11:02 2002 Page 3

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