GC/MS analysis report for sample AE06410, May 3 2002

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Data File C:\MSDCHEM\l\DATA\020409\6410.D Vial: 14 Acq On 10 Apr 2002 3:16 am Operator: McLean Sample 3/18 Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e Quant Method : C : \MSDCHEM\1. . .\SC7\NAPR0902 .M (Chemstation Integrator) Title : Method 508 GC/MS Scan Library : C:\DAT7kBASE\nist98.1 ********************************************************************* Peak Number 1 Acetonitrile, dichloro- Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T. 3.32 0.31 ug/1 241469 1,4-Dichlorobenzene-d4 10.67 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Acetonitrile, dichloro- 109 C2HC12N 003018-12-0 78 2 Acetonitrile, dichloro- 109 C2HC12N 003018-12-0 56 3 1-Propyne, 3-chloro- 74 C3H3C1 000624-65-7 5 4 1-Propyne, 3-chloro-_________________ 74 C3H3C1 000624-65-7 5 Abundance Scan 41 (3.320 min): 6410.D (-35) (-) Wz 74700 100700% 7)4

5000 82 47 3.20 3.30 3.40 3.50 3.60 3.70 40 ' .1 ' ' ' ' I ' ' ' ' I ' ' ' ' I ' ' ' ' I ' ' ' ' I ' ' ' ' I ' ' m/z 82.00 41.31% ■n/z-> 10 20 30 40 50 60 70 80 90 100 110 Abundance #28338: Acetonitrile, dichloro-

5000 82 3.20 3.30 3.40 3.50 3.60 3.70 47 m/z 76.00 33.68% 35 12 26 I,Il , ,i|i|,, , 108 v/z-> 10 20 30 40 50 60 70 80 90 10O 110 Abundance #115342: Acetonitrile, dichloro-

35 .11........ 3.20 3.30 3.40 3.50 3.60 3.70 5000 82 “m/z 84.00 25.39% 47

' I ' ' ' ' I ‘ ' I ' ' ' ' I ' ' ' ' I ‘ ' I ' •n/z-> 10 20 30 40 50 60 70 80 90 100 110 Abundance #108401:1-Propyne, 3-chloro- p ‘' I 30 2203J0340a50a60370 m/z 47.05. 24.13% 5000

at. 74

V 57 h-r-r^ ■nZz-> 10 20 30 40 50 60 70 80 90 100 110 3.20 3.30 3.40 3,50 3.60 3.70

6410.D SC7\NAPR0902 .M Thu May 02 14:15:32 2002 Page 3

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