DEP water sample drip rate log, June 2002

NYC 9/11 Public Portal Document Library searen compound Report Data File C:\MSDCHEM\1\DATA\060602\603LB.D Vial: 3 Acq On 6 Jun 2002 12:57 pm Operator: McLean Sample 6/3 eh Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e Quant Method : C:\MSDCHEM\1\METHODS\060302.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L Peak Number 9 Morpholine Concentration Rank 3

R.T. EstConc Area Relative to ISTD R.T.

4.11 1.41 ug/L 1098160 1,4-dichlorobenzene-d4 9.89

Hit# of 5 Tentative ID MW MolForm' CAS# Qual 1 Morpholine 87 C4H9NO 000110-91-8 9 2 Glycine, methyl ester 89 C3H7NO2 000616-34-25 3 Morpholine 87 C4H9NO 000110-91-8 4 4 2-Propenenitrile, 2-chloro- 87 C3H2C1N 000920-37-6 4 Abundance Scan 175 (4.107 min): 603LB.D (-171) (-) m/ z 87.05Z 100.00% 87

55 5000 43 38 1 AnAi.“Anhsa.byq 48 3.80 4.00 4.20 4.40 Of ----- - • ‘ ‘ >i'*• • i ■i “ ‘ ‘‘‘i1 ‘1 * i i “ ■ ■ i ■11 ■ i m/z 89.00 99.88% niz-> 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 Abundance #108086: Morpholine 29 57 87

5000 3.80 4.00 4.20 4.40 m/z 55.10 63.67% ..... 15.24, ,34..1147.,52. ,63 70 77 82 Ot " i ■1'11" ■11"111" " i11 1111"11"' '1'"' i '■'' I'I HT nz-> 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 Abundance #36033: Glycine, methyl ester 89 < ■ । • i i 3.80 4.00 4.20 4.40 5000 m/z / 86.00 41.24% 44 59

n/z-> o! 5 a4 54 , |, 66 TIHtgt Tpm 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 Abundance #473: Morpholine 29 57 ‘ 3,80 4.00 4.20 4.40 m/z 43.10 39.72% 87

MMMw"W 5000

42

n/z-> 0 1 • i' ‘" i1 ■ “ 111111111111 +37+14+——62+ 62 68 73 78 1TTgt 1 ■ i *1 ■ 11 ■ ■ ■ 11 1 ‘ ■ I ‘ ‘ 1 I 1 I ■ 1 I I I > /1 *CI 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 3.80 4.00 4.20 4.40

603LB.D 060302.M Mon Jun 10 10:20:45 2002 Page 12

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