GCMS analysis results for sample AE12327, June 2002

NYC 9/11 Public Portal Document Library searen Compound Report

Data File : C:\MSDCHEM\1\DATA\052802\12327.D Vial: 7 Acq On : 28 May 2002 7:11 pm Operator: McLean Sample : 5/24 ad Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e Quant Method : C:\MSDCHEM\1\METHODS\052202.M (Chemstation Integfator) Title : 508 Modified GC/MS scan *= Library : C:\DATABASE\NIST98.L ********************************************************************* Peak Number 5 Propiolonitrile Concentration Rank 6 R.T. EstConc Area Relative to ISTD R.T. 3.99 1.87 ug/L 1031720 1,4-Dichlorobenzene-d4 9.90 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Propiolonitrile 51 C3HN 001070-71-9/3 2 Ethanol, 1-ethoxy-2,2,2-trifluoro- 144 C4H7F3O2 000433-27-/2 3 Ethanethiol, 2-amino-, hydrochlo... 113 C2H8C1NS 000156-57-0 1 4 Pyrrolidine, 2-ethyl-1-methyl- 113 C7H15N 026158-82-7 1 Abundance Scan 155 (3,990 min): 12327.D (-154) (-) m/z / 47.10 100.00% 47 84

50001

58 3.60 3.80 4.00 4.20 440 nz-> o! mp, 4 10 20 30 40 50 L......... 11 ■1 ‘ ■ I ■1 ‘' i ■ 60 70 80 90 100 110 120 130 m/z 51.00 74.49% Abundance #12371: Propiolonitrile 51

5000 3.60 3.80 4.00 4.20 4.40 m/z _ 84.00 72.82% 12 io 25 . 38 0! -118.13211) +*1991W91mmmRTTT n/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 Abundance #12277: Ethanol, 1 -ethoxy-2,2,2-trifluoro- 47 3.60 3.80 4.00 4.20 4.40 5000 m/z 48.10 22.44% 75 69 ,82 99 115 127 01 11 1111 ■■•■।■1 i ■ ■ ■ • i ■ ■ ■ ■ i ■ ■ ■■ i ■ ■ n/z—> 10 20 30 40 50 60 70 80 90 100 110 120 130 Abundance #715: Ethanethiol, 2-amino-, hydrochloride 33 3.60 3.80 4.00 4.20 4.40 36 m/z 43.10 16.03% 5000

42 59 ApMMwoahnyiopat 15 77 o- - +L30 l4ll48— 70 n/z—> 10 20 l 40 50 ' 60 70 80 90 100 110 120 130 3.60 3.80 4.00 4.20 4.40

12327.D 052202.M Thu May 30 10:41:10 2002 Page 7

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