GCMS analysis results for sample AD31644, Jan 28 2002

NYC 9/11 Public Portal Document Library searen compound Report Data File : C:\MSDCHEM\1\5973N\02JAN17\31644.D Vial: 4 * Acq On : 17 Jan 2002 5:19 pm Operator: Sample : 508 scan Inst : Instrumen Mise : January 17, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\SCAN508.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 8 2-Propanol, 1- (2-methoxypro. . . Concentration Rank 3 R.T. EstConc Area Relative to ISTD R.T. 9.84 0.33 ug/L 132973 1,4-Dichlorobenzene-d4 9.71 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 2-Propanol, 1-(2-methoxypropoxy)... 148 C7H16O3 013429-07-7 83 2 TRIPROPYLENE GLYCOL 2 192 C9H20O4 000000-00-0 43 3 3-Hexanol 102 C6H140 000623-37-0 40 4 Methane, diethoxy- $$ Ethane, 1,... 104 C5H1202 000462-95-3 9 Abundance Scan 566 (9.836 min): 31644.D (-) m/z 59.10 100.00% 59

5000

0- ........ mj .... 45 1,1 73 104■ i1 ■ ■ ■ i ■ ■ ■ ■ i ■ ■ ■ ■ i''''' i • ■ ■ • i ■ ‘1 • i ■ ■ ■ ■ i1 ■ ■ • i ■ ■ ■ ■ i ■ ■ ■ ‘ i _M_ 9.40 m/z 9.60 TTrrfrer 9.80 10.00 10.20 12.21% m/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160

UA Abundance #43942:2-Propanol, 1-(2-methoxypropoxy)-$$ 1-(2-Methoxyp... 59

5000 ‘ I** 9.40 9.60 9.80 10.00 10.20 m/z 43.10 8.96% 31 45

niz-> 0-’......... | T—tt • i • 20 30 ..40l ,svselpans ...................... . 50 60 70 80 90 100 110 120 130 140 150 160 Abundance #102327: TRIPROPYLENE GLYCOL 2 50 9.40 9.60 9.80 10.00 10.20 5000 m/ z 73.10 8.95% 103

MA 45

miz-> 0- — ... I.., -72 ..... . 117 130 161 111. >. J. I I»j I I .. I. 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 i ■ •1 ■ I •1 ■ ■ i ■ ■ • • i • ■ ■ • i ■ ■'11

Abundance #9539:3-Hexanol — 53 9.40 9.60 9.80 10.00 10.20

N/ m/z 41.10 8.80% 31 5000 43 73

miz—> 0 —20mp 44—— —mm 30 40 50 60 70 80 90 100 110 120 130 140 150 160 !8.8 9.40 9.60 9.80 10.00 10.20

31644.D SCAN508.M Tue Jan 22 08:37:18 2002 Page 10

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