GCMS analysis results for sample AE00105, Feb 2002

Machine-extracted title · confidence 100%

Laboratory report listing unknown compounds and surrogate recovery for sample AE00105 analyzed on February 7, 2002.

NYC-WTC_000050793–000050812

Folder label: “GCMS X 1/4/02 A 1/25/02”

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NYC 9/11 Public Portal Document Library searen compound Keport

Data File : C: \MSDCHEM\1\5973N\02JAN25\00105.D Vial: 3 ’ Acq On : 25 Jan 2002 11:49 am Operator: Sample : 508 scan Inst : Instrumen Mise : January 25, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\l..-\SCAN508.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 9 2-Propanol, 1-(2-methoxy-l-... Concentration Rank 5

R.T. EstConc Area Relative to ISTD R.T.

9.63 0.21 ug/L 88678 1,4-Dichlorobenzene-d4 9.71

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 2-Propanol, 1-(2-methoxy-1-methy... 148 C7H16O3 020324-32-7 83 2 DIPROPYLENEGLYCOL METHYL ETHER $... 148 C7H16O3 020324-32-7 56 3 2-[(Methoxyethoxy)ethoxy)ethyl] ... 280 C13H2806 000000-00-0 56 4 2-Butanol, 3,3‘-oxybis-__________ 162 C8H18O3 054305-61-2 50 Abundance Scan 548 (9.630 min): 00105. D (-) m/z 59.10 100.00% 59

5000 45 73 103

9.20 9.40 9.60 9.80 10.00 • i ■ ■ • ■ i ■ ■ ■' i ■ W.... Il.... —P 86 m/ z 45.10 42.47% m/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 Abundance #43943:2-Propanol, 1-(2-methoxy-1 -methylethoxy)- $$ Dipro... 59

5000 ■ i ■ ■ 45 103 9.20 9.40 9.60 9.80 10.00 73 31 m/z 103.10 34.16%

m/z-> ■ • i ■ -I------- T 130 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 • l • • • ’ I * i • ■ ■ ■ i ■ i • • ■ ■ i

Abundance #43944: DIPROPYLENEGLYCOL METHYL ETHER $$ 2-Propanol, 1-(2... 59 103 I D ■ 1

9.20 9.40 9.60 9.80 10.00 5000 m/z 73.10 29.45% 45 73 31

n/z-> Abundance 10 —— 20 1 r 1111111111 30 40 50 60 70 80 90 100 110 120 130 TT 130 i ■ • • ■ i ’

#225155:2-[(Methoxyethoxy)ethoxy)ethyl] 2-[(2"-hydrox... 59 i • • ■ ■ i 140 150 . MA, 9.20 9.40 9.60 m/ z 41.00 9.80 10.00 17.15% 5000 45 9.60 .

Tl/Z-> 31

'T111' 11 ■ ' ■i '''' r 1 10 20 30 40 50 + 60 73 TPPTT 89

70 80 90 103 | 117 ++ 100 110 120 130 140 150 133 I’ll 11......... । > 1111 h... ।। 147

9.20 9.40

00105.D SCAN508.M Mon Jan 28 09:49:48 2002 Page 11

NYC-WTC_000050807

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