GCMS analysis results for sample AD31638, Jan 28 2002

NYC 9/11 Public Portal Document Llbrary searen compound keport

Data File : C:\MSDCHEM\1\5973N\02JAN17\31638.D Vial: 5 ’ Acq On : 17 Jan 2002 1:32 pm Operator: Sample : 508 scan Inst : Instrumen Mise : January 17, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\SCAN508 .M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 4 Acetic acid, 3-[1,3]dioxola... Concentration Rank 1 R.T. EstConc Area Relative to ISTD R.T. 5.89 3.70 ug/L 1167900 1,4-Dichlorobenzene -d4 9.72 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Acetic acid, 3-[1,3]dioxolan-2-y... 174 C8H14O4 000000-00-0 33 2 3-(CYCLOHEX-3'-EN-YL)PROPANOL $$... 174 C8H14O4 015745-87-6 33 3 Silane, tetramethyl- 88 C4H12Si 000075-76-3 9 4 N-Ethylformamide $$ N-Formylethy... 73 C3H7NO 000627-45-2 9 Abundance Scan 220 (5.885 min): 31638.D (-) m/z 73.10 100.00% 73

5000 43 5.60 5.80 6.00 6.20

miz-> 0- .1 1 55 mmmpmpm .1 1.87,1111193. ... ..... 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 m/z 43.10 25.63% Abundance #78238: Acetic acid, 3-[1,3]dioxolan-2-ylpropyl ester 73

T J l 1 i * — 4 . rr > 5000 TTE 5.60 5.80 6.00 6.20 43 m/z 41.10 9.58% 27 55 . , 87 113 । . . . . । . , । > i . . । . . . . । . . . . ।174 iz-> 0- u i • ■■ ■ i “ " i' upBapuBosgommap 'I . . । . I'l | . . > . ( . . . . । 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 .I.l|>

Abundance #36138:3-(CYCLOHEX-3'-EN-YL)PROPANOL $$ 2-Cyclohexene-1-p... 73 1 1 T’tT 5.60 5.80 6.00 6.20 5000 m/z 45.10 9.56% 43 27 87 miz-> 0- 55 mpnpmm; +pn i ‘ i"' ‘i 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 113 174 ■11 ■1 ■ 'i *'" i‘ ■ ‘ ■ i1 “11 “ ■ ■ i ■i‘

Abundance #4814: Silane, tetramethyl- • ‘ i ‘ ‘ ‘ ‘ i * ‘ ‘ ‘ I ‘ ‘ 1 ‘ I ‘ ‘ 73 5.60 5.80 6.00 6.20 m/z 71.10 6.31%

5000-

45 15 , ,1 53. 0- TDTmp 88 “IIUmumumn—mnum—TT’ • I • ■ T ■ l • iz—> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 5.60 5.80 6.00 6.20

31638.D SCAN508.M Tue Jan 22 08:37:02 2002 Page 6

NYC-WTC_000049953