Gas chromatography-mass spectrometry analysis of sample AE00327 showing unknown compounds and surrogate 2,4-DDD measurement.
NYC-WTC_000051192–000051205Folder label: “GCMS X 1/8/02 A 1/10/02”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document
Llprary searcn compound Keporc Data File : C:\MSDCHEM\1\5973N\02JAN10\00472.D Vial: 7 ‘ Acq On 10 Jan 2002 7:46 pm Operator: Sample : 508 scan ext 1/8 Inst : Instrumen Mise : January 10, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\SCAN508. M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L
Peak Number 5 3-(CYCLOHEX-3'-EN-YL)PROPAN... Concentration Rank 1 R.T. EstConc Area Relative to ISTD R.T. 5.89 4.40 ug/L 1504370 1,4-Dichlorobenzene-d4 9.71 Hit# of 5 Tentative ID MW MolForm CAS# Qual
13-(CYCLOHEX-3 ′ -EN-YL)PROPANOL $$. . . 174 C8H14O4 015745-87-6 33 2 Acetic acid, 3-[1,3]dioxolan-2-y... 174 C8H14O4 000000-00-0 33 3 Silane, tetramethyl- 88 C4H12Si 000075-76-3 25 4 Silane, tetramethyl- $$ Tetramet... 88 C4H12Si 000075-76-3 9 Abundance Scan 220 (5.885 min): 00472.D (-) m/z 73.10 100.00% 73
5000
43 5.60 5.80 6.00 6.20
n/z-> 01 TPPP 17,1,15%... ,'1.11 .... 87..... 103......................... ' ■ i ■ ■ ■ ■ i ■ ■ ■' i ■' ■ i' ■ ■' i ■' ■
10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 • ■ i' ■ ■ i ■'1 r i ■ TTT m/z 43.10 24.00% Abundance #36138: 3-(CYCLOHEX-3'-EN-YL)PROPANOL $$ 2-Cyclohexene-1-p... 7)3
5000 5.60 5.80 6.00 6.20 43 m/z 41.10 9.30%
o1mPTTm27 ... 55 ! . i , T1 87 113 174 m/z-> 10 20 30 40 50) 60 70 80 90 100 110 120 130 140 150 160 170 180 Abundance #78238: Acetic acid, 3-[1,3]dioxolan-2-ylpropyl ester 73
5.60 5.80 6.00 6.20 5000 m/z 45.10 9.24% 43
m/z-> Abundance 27 55 ,I 01■ ■ r ' " i1 ‘' r TTT 11" ' ‘ i " r 'T' 87 113 1 " i " 1' i'1'111 ’ ■ ■ i 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 #4814: Silane, tetramethyl- 174 " i " " 11' " i" 1' I " " i'1111'1" ir . ' IN ''' I ' ' 1 ' 7)3 5.60 5.80 6.00 6.20 m/z 71.10 6.35%
5000
45 | 53 15 0 TTITTT ।11111,11 I 88 111' 11 1 ’' i " ■' i • " 11" " i1" 11'11' i1" ■ i'' " i' " ' i11" i' ■ ■' r 10 m/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 5.60 5.80 6.00 6.20
0472.D SCAN508.M Fri Jan 11- 10:08:55 2002 Page 7
NYC-WTC_000051200
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Ranked by indexed similarity. Reasons describe shared subjects and filing context; check the source records.
NYC-WTC_000051088
Laboratory report showing GCMS analysis of sample AE00309 for unknown compounds and DDD on January 10, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.994
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000051055
Laboratory report showing GCMS analysis of sample AE00307 for unknown compounds and DDD on January 10, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.994
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000051422
Laboratory report showing GCMS analysis of sample AE00463 with surrogate recovery data on January 24, 2002.
1 shared topics · Same agency, volume and box · similarity 0.993
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000051105
Laboratory report showing GCMS analysis of sample AE00318 for unknown compounds and DDD on January 10, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.993
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000051301
Laboratory report showing GCMS analysis of sample AE00471 with surrogate recovery data on January 18, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.993
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000051408
Laboratory report showing GCMS analysis of sample AE00462 with surrogate recovery data on January 24, 2002.
1 shared topics · Same agency, volume and box · similarity 0.993
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000050793
Laboratory report listing unknown compounds and surrogate recovery for sample AE00105 analyzed on February 7, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.992
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000049929
Laboratory report showing GCMS analysis of sample AD31637 including unknown compounds and surrogate recovery data.
2 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.992
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000051439
Laboratory report showing GCMS analysis of sample AE00464 with surrogate recovery data on January 24, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.992
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000051073
Laboratory report showing GCMS analysis of sample AE00308 for unknown compounds and DDD on January 10, 2002.
1 shared topics · Same agency, volume and box · similarity 0.992
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000049990
Laboratory report showing GCMS analysis of sample AD31644 including unknown compounds and surrogate recovery data.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.991
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000006045
Analytical report showing surrogate recovery data for sample AE03184 analyzed on March 15, 2002.
1 shared topics · similarity 0.992
machine-extracted · confidence unavailable · Check page ↗Similar subjects in other documents. Similarity does not establish the same event, measurement or conclusion.
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NYC-WTC_000051152
Administrative record from DEP Box 28 documenting GCMS activities at the World Trade Center site in January 2002.
Filed in the same folder
NYC-WTC_000051153
Document header page containing identification codes and metadata for GCMS files processed in early January 2002.
Filed in the same folder
NYC-WTC_000051156
Laboratory report detailing GCMS analysis of sample AE00327 for volatile organic compounds on January 10-11, 2002.
Filed in the same folder
NYC-WTC_000051165
Laboratory report showing GCMS analysis of reference standards used for calibration during January 10-11, 2002 testing.
Filed in the same folder
NYC-WTC_000051179
Laboratory report documenting GCMS blank analysis to verify system cleanliness during January 10-11, 2002 testing.
Filed in the same folder