GCMS results for sample AE00464, Jan 24 2002

NYC 9/11 Public Portal Document Llprary Search Compound Report

Data File : C:\MSDCHEM\1\5973N\02JAN11\00464.D Vial: 6 Acq On : 11 Jan 2002 6:15 pm Operator: Sample : 508 scan Inst : Instrumen Mise : January 11, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\MSDCHEM\1...\SCAN508. M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L

Peak Number 4 3-(CYCLOHEX-3'-EN-YL)PROPAN... Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T.

5.89 4.45 ug/L 1416710 1,4-Dichlorobenzene-d4 9.72

Hit# Of 5 Tentative ID MW MolForm CAS# Qual

13-(CYCLOHEX-3'-EN-YL)PROPANOL $$... 174 C8H14O4 015745-87-6 33 2 Acetic acid, 3-[1,3]dioxolan-2-y... 174 C8H14O4 000000-00-0 33 3 Silane, tetramethyl- $$ Tetramet... 88 C4H12Si 000075-76-3 25 4 Silane, tetramethyl- (CAS) $$ Te... 88 C4H12Si 000075-76-3 9 Abundance Scan 220 (5.885 min): 00464.D (-) m/ z 73.10 100.00% 73

•n/z-> 5000

0 10 I I 55 pmmmmmmT— . 87 11’..... 1 43

20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 103 r ■ ■ ■ i 1 5.60 5.80 6.00 6.20 m/z 43.10 24.79% Abundance #36138: 3-(CYCLOHEX-3'-EN-YL)PROPANOL $$ 2-Cyclohexene-1-p... 78

A . J V___ _ 5000 5.60 5.80 6.00 6.20 43 m/z 41.10 9.82% 27 55 .i 87 113 174 0 ■ i ■' ■' i'' ■ ■ i1 . ........ . i ■ ’ ■ • i ’ I.... 1 I i''' ■ i''1 ■ i'''' i' " ' r ' " i' " ' r ' ■' i v Tl/Z--> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 Abundance #78238: Acetic acid, 3-[1,3]dioxolan-2-ylpropyl ester 73 1111 / 11 — 1 । । "i rr,

5.60 5.80 6.00 6.20 5000 m/z 4 5.10 9.44% 43 27 87 113 ■ " i " ■ j ■ +prr ■" i''' ■ i' " ■ i" 1' i' " ■ i ■ ■'' i ■ " ' i1 ■'' i ■ " ' r 0^ T+ ■ r55 174 i ■ "■ i m/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 Abundance #4812: Silane, tetramethyl- $$ Tetramethylsilane $$ (CH3)4... 73 5.60 5.80 6.00 6.20 m/z 71.10 6.64% 5000

■n/z-> 0 15 r 1" i 31 45 |i•• i>• 88 11'-1" |1I | 55 ■l ><i■"• i■i■••■i• • ■ • i>< i■ >■ • i•■■ ■ i• •• >i • •• ■ i•

10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 —A 5.60 5.80 6.00 6.20

00464.D SCAN508.M Mon Jan 14 10:47:01 2002 Page 6

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