DEP GCMS data table, Jan-Feb 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\MSDCHEM\1\5973N\02FEB27\02383.D Vial: 4 Acq On : 27 Feb 2002 1:13 pm Operator: Sample : 508 scan Inst : Instrumen Mise : February 2 7, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\l-..\HP022102.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N. L Peak Number 5 3-(CYCLOHEX-3'-EN-YL)PROPAN. .. Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T.

5.95 0.43 ug/L 177436 1,4-Dichlorobenzene-d4 9.72

Hit# of 5 Tentative ID MW MolForm CAS# Qual

13-(CYCLOHEX-3'-EN-YL)PROPANOL $$ . .. 174 C8H14O4 015745-87-6 36 2 Acetic acid, 3-[1,3]dioxolan-2-y... 174 C8H14O4 000000-00-0 36 3 Pentane, 3-methoxy- $$ 1-Ethylpr... 102 C6H140 036839-67-5 9 4 Propane, 2-methoxy-2-methyl- (CA... 88 C5H120 001634-04-4 9 Abundance Scan 228 (5.948 min): 02383. D (-) m/z 73.10 100.00% 73

5000 43

i 55 87 103 5.60 5.806.00 6.20 01-TH-10p—]10—]]mmmmp m/z 43.10 26.18% m/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 Abundance #36138:3-(CYCLOHEX-3'-EN-YL)PROPANOL $$ 2-Cyclohexene-1-p... 73

5000 • ■ । ■ ■ - ■ । ■ > ■ • । ■ > ■ ■ । ■ 5.60 5.80 6.00 6.20 43 m/ z 45.10 8.62% 27 55 87 113 174 0- poadhponii ’’1, 11 " '111'1 ’11 laaatlsytass4vse121sag1411*1*/***11**SI*SI|***I m/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 Abundance #78238: Acetic acid, 3-[1,3]dioxolan-2-ylpropyl ester 73 5.60 5.80 J6.00 ■ ‘ i ■ ■ 1 ■ i ' 6.20 5000 m/ Z 71.00 6.16% 43 27 55 87 113 174 01111 ‘111 ■ TT 11———11TTTT7T —TInwuuamtmimnOOTML m/z—> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 Abundance #9698: Pentane, 3-melhoxy- $$ 1-Ethylpropyl methyl ether 73 5.60 5.80 6.00 6.20 m/z 69.00 5.24%

5000 45

27 55 0 pond ' 'i । ■ 10—00—]] m/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 5.60 5.80 6.00 6.20

32383.D HP022102.M Thu Feb 28 08:46:56 2002 Page 7

NYC-WTC_000004996