NYC-WTC_000051088
Laboratory report showing GCMS analysis of sample AE00309 for unknown compounds and DDD on January 10, 2002.
1 shared topics · Same agency, volume and box · similarity 0.992
machine-extracted · confidence unavailable · Check page ↗Document / 13 pages
GCMS blank analysis results for sample AE00327, Jan 2002
Machine-extracted title · confidence 100%Laboratory report documenting GCMS blank analysis to verify system cleanliness during January 10-11, 2002 testing.
NYC-WTC_000051179–000051191Folder label: “GCMS X 1/8/02 A 1/10/02”
Page image
OCR text
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document
ulorary Searcn compound Keporc
Data File : C:\MSDCHEM\1\5973N\02JAN10\0108B.D Vial: 1 ' Acq On : 10 Jan 2002 12:21 pm Operator: Sample : lab blank ext 1/8 Inst : Instrumen Mise : January 10, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\SCAN508.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 1 Cyclobut-l-enylmethanol Concentration Rank 5 R.T. EstConc Area Relative to ISTD R.T. 4.85 0.12 ug/L 38311 1,4-Dichlorobenzene-d4 9.71 Hit# of 5 Tentative ID MW MolForm CAS# Qual
1 Cyclobut-l-enylmethanol 84 C5H80 000000-00-0 9 2 l-Hexene, 6-bromo- 162 C6HllBr 002695-47-8 9 3 4-Pentenal (CAS) $$ 4-Pentenal- 84 C5H8O 002100-17-6 9 4 2-Butenal, 2-methyl- $$ Crotonal... 84 C5H80 001115-11-3 7 Abundance Scan 129 (4.846 min): 0108B.D (-) m/ z 84.00 100.00% 84 5000 41 55
MA
4.40 4.60 4.80 L 5.00 5.20 0- 111"' >11 • ll _ TTTtTEITT‘ETE‘‘TTTTTTTTTT m/ z 55.10 74.30% 1 i' 1 ' ■ i ■ n/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 Abundance #3313: Cyclobut-1-enylmethanol 55
83 27 39 5000 4.40 4.60 4.80 5.00 5 20 m/z 59.00 62.59% 1 66 01.11. .111111'| 111 ’I’ I,.. 1 1 111'1111 1 11 m/z-> 20 30 40 50 60 70 80 90 ' 100 110 120 130 140 150 160 170 Abundance #61496:1 -Hexene, 6-bromo- 41
83 । ' 1 1 1 i ■ ' 1 1 1 1 1 1 1 r1 1 1 1 r 1 1 ' 4.40 4.60 4.80 5.00 5.20 5000 m/ z 41.10 48.17% 27 67
0 .... . 1 , 136 162 n/z-> Abundance ' i1 ■' ■ i''1 ‘ 1111' 11 ' 'T‘'■• । ' ■ ■ ■ । 'I FITTTTTrI ruu r । , iii ।-i I I i (tt > > |ri i T| I I i i । i 20 30 40
41 50 60 70 80 90 100 110 120 130 140 150 160 170 #3208: 4-Pentenal (CAS) $$ 4-Pentenal- 4.40 AN 4 460 4.80 5.00 5.20 m/ z 39.10 42.94% 5000
83 69
m/z—> O' i mmmmir n ■ Mi 20 30 40 50 I 60 70 80 mmmmm-mmmm 90 100 110 120 130 140 150 160 170 i ■ 1 '1 r11 1 1 i 440 4.60 4.80 1 ' I 1 1 rr l r > 5.00 5.20
108B.D SCAN508.M Fri Jan 11 10:09:14 2002 Page 3
NYC-WTC_000051184
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NYC-WTC_000051184Source: NYC Law Department, mirrored locally
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