GCMS analysis results for sample AD31644, Jan 28 2002

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Data File : C:\MSDCHEM\1\5973N\02JAN17\31644.D Vial: 4 • Acq On : 17 Jan 2002 5:19 pm Operator: Sample : 508 scan Inst : Instrumen Mise : January 17, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\SCAN508.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 5 3-(CYCLOHEX-3'-EN-YL)PROPAN... Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T.

5.89 4.51 ug/L 1819740 1,4-Dichlorobenzene-d4 9.71

Hit# Of 5 Tentative ID MW MolForm CAS# Qual

1 3-(CYCLOHEX-3'-EN-YL)PROPANOL $$... 174 C8H14O4 015745-87-6 36 2 Acetic acid, 3-[1,3]dioxolan-2-y... 174 C8H14O4 000000-00-0 36 3 Acetamide, N-methyl- $$ Methylac... 73 C3H7NO 000079-16-3 9 4 Silane, tetramethyl- (CAS) $$ Te... 88 C4H12Si 000075-76-3 9 Abundance Scan 220 (5.885 min): 31644.D (-) m/ z 73.10 100.00% 73

5000 43 r 11 ■ ■' n 1 (। ■ 6.20 niz-> 0 ml . 87 103 I.. p.. i p... p'i.. ( 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 i •' ■ ■ i •' ■ ■ i • ■ “ i'1 ‘11 •' “ i ■ * ■' i m/z 5.60 5.80 43.10 6.00 23.03% Abundance #36138:3-(CYCLOHEX-3'-EN-YL)PROPANOL $$ 2-Cyclohexene-1-p... 73

5000 r' i ■ ■ 1 ■ I ■ ' ■ ■ i 1 ■ ■ • i ■ • 5.60 5.80 6.00 6.20 43 m/z 45.10 8.99% 27 . 55 i , 87 113 174 0- ‘ ■ i ■ ■ ■ ■ i ‘ ■11 ■ ■ ■ ■ । 1 i । । । . i'. । । . । . i'i . 'I.. t.. r. ।।, .-i।।।।।।।. m/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 Abundance #78238: Acetic acid, 3-[1,3]dioxolan-2-ylpropyl ester 73 5.60 5.80 6.00 6.20 5000 m/z 41.10 8.63% 43 27 55 87 113 174 Tpr 1’211111071"Hp 0- 1 miz-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 Abundance #1790: Acetamide, N-methyl- $$ Methylacetamide $$ Monometh... PIu-nek 43 73 5.60 5.80 6.00 6.20 30 m/z 71.10 6.35% 58 5000

15 0 I i ’ ’’I 47++ p..'pIHp...p... p...p...p...p... pPl|....p...p..>p ’ ' I ‘ ‘ 1 ' I ' ‘ ' 1 ‘ ‘ ‘ 1 ' ' iz-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 5.60 5.80 6.00 6.20

31644.D SCAN508.M Tue Jan 22 08:37:18 2002 Page 7

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