GCMS analysis results for sample AD31644, Jan 28 2002

NYC 9/11 Public Portal Document Llbrary aearen compound Keporc

Data File : C: \MSDCHEM\1\5973N\02JAN17\31644.D Vial: 4 • Acq On : 17 Jan 2002 5:19 pm Operator: Sample : 508 scan Inst : Instrumen Mise : January 17, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\SCAN508.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 6 2-Propanol, 1-(2-methoxy-1-... Concentration Rank 6 R.T. EstConc Area Relative to ISTD R.T. 9.54 0.18 ug/L 73633 1,4-Dichlorobenzene-d4 9.71 Hit# Of 5 Tentative ID MW MolForm CAS# Qual 1 2-Propanol, 1-(2-methoxy-1-methy... 148 C7H16O3 020324-32-7 74 2 DIPROPYLENEGLYCOL METHYL ETHER $... 148 C7H1603 020324-32-7 72 3 BIS(1-METHYL-2-HYDROXYETHYL)ETHER 134 C6H14O3 000000-00-0 39 4 2-Butanol, 3,3’-oxybis- 162 C8H18O3 054305-61-2 39

A Abundance Scan 540 (9,539 min): 31644.D(-) m/z 59.10 100.00% 50

5000 45 103 73 ■ ■ i ■ ■ ' ■ I ' ■ 1 ' 1 ‘ ‘ ‘ f 1 1 1 1 1 1

84 9.20 9.40 9.60 9.80 niz-> 0- — .... ill,.. 'I 10 20 30 40 50 60 70 80 i ■ ■ ■ • i1 • ■ ■ i ■1 ■ > i ■ ■ •11 ■ ■ • I ' ' ‘ ' I ' ' ‘ ■ I' ' ‘ ' I ‘ 100 110 120 130 140 m/z 45.10 42.44% Abundance #43943:2-Propanol, 1-(2-methoxy-1-methylethoxy)- $$ Dipro... 50

5000 45 103 9.20 9.40 9.60 9.80 73 31 m/z 103.10 40.12% 01 . . Mm IT. ■ 1 ‘ ■ i • ■ ■ ■ i ■1 ■ ■ i ■ ■ •' i ■ • ■ ■ I ■ ■ • ■ i • nfz~> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 Abundance #43944: DIPROPYLENEGLYCOL METHYL ETHER $$ 2-Propanol, 1-(2... 59 103 *1***1**’*I’I’*I* 9.20 9.40 9.60 9.80 5000 m/z 73.10 26.86% 45 73 31 15 , t 130 0- ■' i ■ ■ i' ■ ■ ■ i 1111 --+---*-Tp ■ ■ i' ■ ■ ■ i ■ ■ ■ • I ■ ■ ■11 ■ • ■ 11 mfz-> Abundance 10 20 30 40 50 60 70 80 90 100 110 120 130 140 #29208: BIS(1-METHYL-2-HYDROXYETHYL)ETHER 50 9.20 AM M9.40 9.60 9.80 m/z 41.10 22.51%

mz—> 5000 31

0 " I " ' i'| i i ib | i i > i । ih H 10 20 30 40 50 45

T+ BupBnTTIT 60 70 80 90 103

134 i ‘ • t • ■ • • i • ■ * ■ i ■ * • * i * 100 110 120 130 140 ■ A.. I ■ i ■

9.20 9.40 ■ ■ ■ i ■ ‘ ML 9.60 9.80

31644.D SCAN508.M Tue Jan 22 08:37:18 2002 Page 8

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