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GCMS analysis results for sample AE06797, April 2002

Machine-extracted title · confidence 100%

Laboratory report documenting GCMS analysis of environmental sample AE06797 conducted on April 19, 2002.

NYC-WTC_000039986–000039994

Folder label: “GCMS X 3/21/02 A 4/16/02

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OCR text

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NYC 9/11 Public Portal Document Llbrary searcn compound Report

Data File : C:\MSDCHEM\1\DATA\041602\6797.D Vial: 15 . Acq On : 16 Apr 2002 8:10 pm Operator: Bohik Sample : SAMPLE 6797 3/21/02 Inst : Instrumen Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\MSDCHEM\1\5973N\5080402BBC.M (RTE Integrator) Title : Quantitation For Method 508gcscan Library : C : \DATABASE\WILEY7N . L

Peak Number 1 3-(CYCLOHEX-3'-EN-YL)PROPAN... Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T.

5.44 4.05 ug/L 262303 1,4-Dichlorobenzene-d4 9.41

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 3-(CYCLOHEX-3'-EN-YL)PROPANOL $$... 174 C8H14O4 015745-87-6 38 2 Acetic acid, 3-[1,3]dioxolan-2-y... 174 C8H14O4 000000-00-0 38 3 Butane, 2-methoxy-2-methyl- $$ E... 102 C6H14O 000994-05-8 36 4 N-Ethylformamide $$ N-Formylethy... 73 C3H7NO 000627-45-2 9 Abundance Scan 401 (5.435 min): 6797.D (-) m/z 73.10 100.00% 73

5000

43 5.00 5.20 5.40 5.60 5.80 0 ....... 1,1, i 87 103 m/z 43.10 22.64% m/z— > 20 30 40 50 60 70 80 90 100110120130140150160170180 Abundance#36138: 3-(CYCLOHEX-3'-EN-YL)PROPANOL $$ 2-Cyclohexene-1-p... 73

5000 TTPTIT -—al—* 5.00 5.20 5.40 5.60 5.80 43 m/z 41.10 9.03%

27 55 ! 87 113 131 174 m/z-> 0 ... t . . | " l > 11 n''|'i ।11111''' 111 " i"'' i' i" " r "' r "' r " ■ I" ‘' i ‘1 r' i' ■ 20 30 40 50 60 70 80 90 100110120130140150160170180 Abundance #78238: Acetic acid, 3-[1.3]dioxolan-2-ylpropyl ester 73 AA — I’I ' ■ i ■ 5.00 5.20 5.40 5.60 5.80 5000 m/z 45.10 8.57%

43 27 131 87 +.... h " r'" 113 174 55 _ 0 - 11 — 11 — ■। ।" "Y1 i' r "' i" " r " ■ r "' I" " i" " i" m/z-> 20 30 40 50 60 70 80 90 100110120130140150160170180 Abundance #9702: Butane, 2-methoxy-2-methyl- $$ Ether, methyl tert-p... 73 I’I 5.00 5.20 5.40 5.60 5.80 m/z 71.10 7.68%

5000

43 55 87 29 m/z-> 0 -l I * ■ i ■' >11 20 30 40 50 60 70 80 90 100110120130140150160170180 ।" I"'' l" " I" " I" " i ’ ■ ■ ■ i" ‘' l"'1 >' ■ 5.00 5.20 5.40 5.60 5.80

5797.D 5080402BBC.M Thu Apr 18 18:00:12 2002 Page 3

NYC-WTC_000039993

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NYC-WTC_000039993Source: NYC Law Department, mirrored locally

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