GCMS surrogate recovery data for sample AE06585, April 18, 2002

NYC 9/11 Public Portal Document Library Search Compound Report

Data File : C:\MSDCHEM\1\DATA\041502\6585.D Vial: 9 Acq On : 15 Apr 2002 4:38 pm Operator: Bohik Sample : SAMPLE 6585 3/20/02 Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\MSDCHEM\1\5973N\5080402BBC.M (RTE Integrator) Title : Quantitation For Method 508gcscan Library : C:\DATABASE\WILEY7N.L

Peak Number 1 3-(CYCLOHEX-3’-EN-YL)PROPAN... Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T.

5.43 9.29 ug/L 647556 1,4-Dichlorobenzene-d4 9.41

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 3-(CYCLOHEX-3'-EN-YL)PROPANOL $$... 174 C8H14O4 015745-87-6 39 2 Acetic acid, 3-[1,3]dioxolan-2-y... 174 C8H14O4 000000-00-0 39 3 Silane, tetramethyl- (CAS) $$ Te... 88 C4H12Si 000075-76-3 23 4 N-Ethylformamide $$ N-Formylethy... 73 C3H7NO 000627-45-2 9 Abundance Scan 400 (5.429 min): 6585.D (-) m/z 73.10 100.00%' 73

5000

43 5.00 5.20 5.40 5.60 5.80

m/z-> 0 i 20 ■11 ■ 40 60 ■

80 AX 100 120 140 160 87 180 103 m/z 43.10 21.81%

Abundance#36138: 3-(CYCLOHEX-3'-EN-YL)PROPANOL $$ 2-Cyclohexene-1-p... 73

5000 T 157* i ' ' TTTTTA 5.00 5.20 5.40 5.60 5.80 43 m/z 45.10 8.63%

0 ■ ■ i ■ “ 27 55 ‘ '401 4 — —L 87.. 113 131..... 174 । , I m/z-> 20 60 80 100 120 140 160 180 Abundance #78238: Acetic acid, 3-[1,3]dioxolan-2-ylpropyl ester 73

i * ■ ■ ■ । ■ i ■ ■ TAAAAT 1' 5.00 5.20 5.40 5.60 5.80 5000 m/z 41.10 7.45%

43

27 55 187 ... 113 131.... 174 , 0 ■ ■ i ■ + 1 ' i1 ' ' i 1 1 m/z-> 20 40 60 80 100 120 140 160 180 Abundance #4813: Silane, tetramethyl- (CAS) $$ Tetramethylsilane $$ ... 73 TA-APAAA 5.00 5.20 5.40 5.60 5.80 m/z 71.10 7.30%

5000

45 29

m/z-> 0 15 ' ' l 20 H II 40 55 ‘ 60 । 80 88.......................................................... 100 120 140 160 180 —AH -----PPPP 5.00 5.20 5.40 5.60 5.80

5585.D 5080402BBC.M Wed Apr 17 16:43:40 2002 Page 3

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