GCMS surrogate recovery data for sample AE06586, April 18, 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\MSDCHEM\l\DATA\041502\6586.D Vial: 10 Acq On : 15 Apr 2002 5:27 pm Operator: Bohik Sample : SAMPLE 6586 3/20/02 Inst Instrumen Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\MSDCHEM\1\5973N\5080402BBC.M (RTE Integrator) Title : Quantitation For Method 508gcscan Library : C:\DATABASE\WILEY7N.L

Peak Number 1 Silane, tetramethyl- Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T.

5.42 8.89 ug/L 662756 1,4-Dichlorobenzene-d4 9.41

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Silane, tetramethyl- 88 C4H12Si 000075-76-3 38 2 Acetic acid, 3-[1,3]dioxolan-2-y... 174 C8H14O4 000000-00-0 36 3 3-(CYCLOHEX-31-EN-YL)PROPANOL $$... 174 C8H1404 015745-87-6 36 4 1,3-Dioxolane, 2-pentadecyl- $$ ... 284 C18H36O2 _____ 004360-57-0 3 6 Abundance Scan 399 (5.424 min): 6586.D (-) m/z 73.10 100.00% 73

5000

43 i ■ ■ ■ ■ i 5.00 5.20 5.40 5.60 5.80 87 103 0— ' r I TI1I I ' —55 4 '+ ' i ■ 1 ' ■ i '■ ■ ■ 1 i 1 ' ■ 1 i ■ ' 1 ■ i ' ' ' ■ i ■ m/z 43.10 23.92% m/z—> 0 20 40 60 80 100 120 140 160 180 Abundance #4814; Silane, tetramethyl- 73

5000 —TT 5.00 5.20 5.40 5.60 5.80 m/z 45.10 8.34% 43 2 15 29 55 , 88 0 ■ i ■ ' ' ' i ' TTIf ' i ' 1 ■' i 1 1 ' 1 I 1 1 1 1 I 1 1 1 1 I 1 1 1 1 I r m/z-> 0 20 40 60 80 100 120 140 160 180 Abundance #78238: Acetic acid, 3-[1,3]dioxolan-2-ylpropyl ester 73

I ' ' ' ' 1 1 ' A 5.00 5.20 5.40 5.60 5.80 m/z 41.20 8.30% TIO’r

5000

43

55 , 27 113 131 174 87 0—)T --- । — -------- m/z-> 20 40 60 80 100 120 140 160 180 Abundance#36138: 3-(CYCLOHEX-3'-EN-YL)PROPANOL $$ 2-Cyclohexene-1-p... 73 5.00 5.20 5.40 5.60 5.80 m/z 71.10 6.97%

5000

43 27 „ 55 87 113 131 174 0^ I 4 — —I • ' I 14 1 m/z—> 0 20 40 60 80 100 120 140 160 180 5.00 5.20 5.40 5.60 5.80

6586.D 5080402BBC.M Wed Apr 17 17:32:15 2002 Page 3

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