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GCMS surrogate recovery data for sample AE06585, April 18, 2002

Machine-extracted title · confidence 100%

Surrogate recovery data for sample AE06585 analyzed by GCMS on April 18, 2002.

NYC-WTC_000039796–000039805

Folder label: “GCMS X 3/20/02 A 4/15/02

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Scanned page image, NYC-WTC_000039804
OCR text

OCR status: ok · source: pdftotext

NYC 9/11 Public Portal Document

Library Search Compound Report

• Data File : C:\MSDCHEM\l\DATA\041502\6585.D Vial: 9 Acq On : 15 Apr 2002 4:38 pm Operator: Bohlk Sample : SAMPLE 6585 3/20/02 Inst : Instrumen Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\MSDCHEM\1\5973N\5080402BBC.M (RTE Integrator) Title : Quantitation For Method 508gcscan Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 2 Benzene-1,2,3,4-d4-, 5,6-di... Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T. 10.26 0.95 ug/L 66432 1,4-Dichlorobenzene-d4 9.41 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Benzene-1,2,3,4-d4-, 5,6-dichlor... 150 C6D4C12 002199-69-1 91 2 1,4-Dichlorobenzene-d4 150 C6D4C12 003855-82-1 91 3 1,4-Dichlorobenzene-d4 150 C6D4C12 003855-82-1 86 4 1,2-Dichlorobenzene-d4 $$ Benzen... 15G C6D4C12 002199-69-1 58 Abundance Scan 1222 (10.259 min): 6585.D (-) m/z 150.00 100.00% 150

115

5000

40 52 78

87 "Mtw ■ ' i ' ' ■ ■ i ' ' AN 10.00 10.20 10.40 10.60 0 — m/z 152.00 72.16% i111' i ‘I H111 ’" I" r "' i" " i "I" ) m/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 Abundance #41699: Benzene-1,2,3,4-d4-, 5,6-dichloro- $$ 1,2-Dichloro... 150

5000

an 38 52

। 78

87 115 Maa _ 10.00 10.20 10.40 10.60 m/z 115.10 67.71% 28 m/z~> 0 m2. . ................ 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 Abundance #41701:1,4-Dich!orobenzene-d4 150

“hrhn 4L. 10.00 10.20 10.40 10.60 m/z 7 .10 38.47% 5000 115 52 78

12 28 40 R9 , 87 99| . TH |124 0 ' ' I ' ' ' TH m/z-> Abundance II II| I I II | I! II M ।)’1 TTTTTTTTt ' r tr f r । ' • | T ■ IT 10 20 30 40 50 60 70 80 90 100110 120 130 140 150 160 #41702: 1,4-Dichlorobenzene-d4 150 M Mik.. 10.00 10.20 10.40 10.60 m/z 117.00 34.37%

5000 115 78 52

T)/z-> 0 i" " i —mm mH A 87

10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 . 1. 10.00 10.20 10.40 10.60

6585.D 5080402BBC.M Wed Apr 17 16:43:41 2002 Page 4

NYC-WTC_000039804

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NYC-WTC_000039804Source: NYC Law Department, mirrored locally

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