GCMS surrogate recovery results, sample AE07178, April 25, 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

■ Data File : C:\MSDCHEM\l\DATA\041802\7178.D vial: 15 Acq On : 18 Apr 2002 8:18 pm Operator: Bohlk Sample : FB, SAMPLE 7178 3/27/02 Inst : Instrumen Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method C:\MSDCHEM\l\5973N\5080402BBC.M (RTE Integrator) Title Quantitation For Method 508gcscan Library C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 1 1,2-Dichlorobenzene-d4 $$ B... Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T.

10.26 0.85 ug/L 63358 1,4-Dichlorobenzene-d4 9.41

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 1,2-Dichlorobenzene-d4 $$ Benzen... 150 C6D4C12 002199-69-1 91 2 Benzene-l,2,3,4-d4-, 5,6-dichlor... 150 C6D4C12 002199-69-1 86 3 l,4-Dichlorobenzene-d4 150 C6D4C12 003855-82-1 86 4 l,4-Dichlorobenzene-d4 150 C6D4C12 003855-82-1 58 Aibundance Scan 1222 (10.259 min): 7178.D (-) m/z 150.00 100.00%' 1!i0

5000 52 78 115

1 10.00 10.20 10.40 10.60 m/z 152.00 61.08% 0 I " " I " " I' " ' I " " I " " I m/z->____ 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 Abundance #41700: 1,2-Dichlorobenzene-d4 $S Benzene-1,2,3,4-d4-, 5,6... 150

5000 115 10.00 10.20 10.40 10.60 78 m/z 78.10 47.91% 52 40 87 0 m/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 Abundance #41699: Benzene-1,2,3,4-d4-, 5,6-dichloro- SS 1.2-Dichioro... 150

115 -mMuOm 10.00 10.20 10.40 10.60 5000 52 78 m/z 52.10 46.17%

38 87 12 28Hi JOU 99 l|.

Miu I HI,............ .. 0 . ............... jTrrrp-rrrpTrq- m/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 Abundance #41702: 1,4-Dichlorobenzene-d4 TT-p-r 150 10.00 10.20 10.40 10.60 m/z 115.10 34.94%

5000 115

m/z-> 0 52 78

87

10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 TT+f Ml., .ill, 10.00 10.20 10.40 10.60

7178.D 5080402BBC.M Tue Apr 23 18:34:38 2002 Page 3

NYC-WTC_000060978