GCMS surrogate recovery results, sample AE07112, April 16, 2002

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Library Search Compound Report

. Data File : C:\MSDCHEM\l\DATA\041002\7112.D Vial: 19 Acq On : 11 Apr 2002 4:50 am Operator: Bohllc Sample : SAMPLE 7112 3/27/02 Inst Instrumen Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\MSDCHEM\l\5973N\5080402BB.M (RTE Integrator) Title : Quantitation For Method 508gcscan Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 1 Benzene-1,2,3,4-d4-, 5,6-di... Concentration Rank 3

R.T. EstConc Area Relative to ISTD R.T.

10.25 0.84 ug/L 64507 1,4-Dichlorobenzene-d4 9.41

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 ■Benzene-l,2,3,4-d4-, 5,6-dichlor... 150C6D4C12 002199-69-1 86 2 1,4-Dichlorobenzene-d4 150 C6D4C12 003855-82-1 72 3 1,2-Dichlorobenzene-d4 $$ Benzen... 150 C6D4C12 002199-69-1 47 4 1,4-Dichlorobenzene-d4 150 C6D4C12 003855-82-1 47 Abundance Scan 1221 (10.253 min): 7112.D (-) m/z 150.00 10^700% 1!i0

115 5000 52 76

87 ‘*'77 .............. 10.00 10.20 10.40 10.60

■n/z-> 0 ................. A.. UI... '... Ill.. 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 m/z 115.10 57.97%

Abundance #41699: Benzene-1,2,3,4-d4-, 5.6-dichloro- $S 1,2-Dichloro... 150

115 5000 52 78 ..... - 10.00 10.20 10.40 10.60 m/z 152.00 47.10% 38 87 0 124 ■n/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140150 160 Abundance #41701: 1.4-Dichlorobenzene-d4 150

10.00 10.20 10.40 10.60 mill 115 m/z 76710 36.28%

52 78

0 0^ 99 I''"I""I' hi Tl/z-> Abundance 10 20 30 40 50 60 70 80 90 100 110 120 130 140150 160 #41700:1,2-Dichlorobenzene-d4 $$ Benzene-1.2,3,4-d4-. 5.6... 1$0 m/z I 10.00 10.20 10.40 10.60 52.10 35.55%

5000 115 78

■n/z-> 0 40 w U 7 52

A 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 u Wi.. 10.00 10.20 10.40 10.60

112.D 5080402BB.M Mon Apr 15 17:55:33 2002 Page 3

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