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GCMS blank analysis results, April 17, 2002

Machine-extracted title · confidence 95%

GCMS blank analysis report for sample AE06580 listing compounds with values below detection limits.

NYC-WTC_000060780–000060788

Folder label: “GCMS X 3/25/02 A 4/17/02

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OCR status: ok · source: pdftotext

NYC 9/11 Public Portal Document

Library Search Compound Report

• Data File : C:\MSDCHEM\l\DATA\041702\LBA0417.D Vial: 5 Acq On : 17 Apr 2002 11:53 am Operator: Bohlk Sample : LB 3/25/02 Inst Instrumen Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\MSDCHEM\l\5973N\5080402BBC.M (RTE Integrator) Title : Quantitation For Method 508gcscan Library : C:\DATABASE\WILEy7N.L ********************************************************************* Peak Number 1 Benzene-1,2,3,4-d4-, 5,6-di... Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T.

10.26 0.83 ug/L 64065 1,4-Dichlorobenzene-d4 9.41

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Benzene-l,2,3,4-d4-, 5,6-dichlor... 150C6D4C12 002199-69-1 91 2 1,4-Dichlorobenzene-d4 150 C6D4C12 003855-82-1 91 3 1,2-Dichlorobenzene-d4 $$ Benzen... 150 C6D4C12 002199-69-1 91 4 1,4-Dichlorobenzene-d4 150 C6D4C12 003855-82-1 91 Abundance Scan 1222 (10.259 min): LBA0417.D (-) m/z 150.00 100.00% 1$0

115 5000 78 52

10.00 10.20 10.40 10.60

m/z-> 0 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 u m/z 152.00 52.66%

Abundance #41699: Benzene-1,2,3,4-d4-. 5,6-dichloro- $$ 1,2-Dichloro... 1$0

115 5000 52 78 1 1 I I I , I -,l p p

10.00 10.20 10.40 10.60 m/z 115.10 50.07% 38 87

Tl/z-> Abundance 12 0 "' I ‘' Uuu 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 #41701:1,4-Dichlorobenzene-d4 iSo ' ' I ' ' 10.00 10.20 10.40 10.60 115 m/z 78.10 43.73%

52 78

8," .99 ]. 124 0 ................ Kr Wi m/z-> Abundance 10 20 30 40 50 60 70 80 90 100 110120 130140 150 160 #41700:1,2-Dichlorobenzene-d4 $$ Benzene-1,2,3,4-d4-. 5,6... 1$0 ■ ..,..1.111 10.00 10.20 10.40 10.60 m/z 52.10 35.03%

5000 115

WL 78 52 40 il 0 m/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 10.00 10.20 10.40 10.60

LBA0417.D 5080402BBC.M Mon Apr 22 10:52:15 2002 Page 3

NYC-WTC_000060786

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NYC-WTC_000060786Source: NYC Law Department, mirrored locally

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GCMS blank results, April 2002 · Box DEP Box 57

NYC-WTC_000061180

Gas chromatography mass spectrometry blank analysis report indicating non-detect levels for target analytes.

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