GCMS blank results, April 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

• Data File : C:\MSDCHEM\l\DATA\041802\LBB0418.D Vial: 21 Acq On : 19 Apr 2002 2:03 am Operator: Bohlk Sample : LB 3/28/02 Inst Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\MSDCHEM\l\5973N\5080402BBC.M (RTE Integrator) Title : Quantitation For Method 508gcscan Library : C:\DATABASE\WILEY7N.L ★w******************************************************************* Peak Number 1 Benzene-1,2,3,4-d4-, 5,6-di... Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T.

10.25 1.06 ug/L 62121 1,4-Dichlorobenzene-d4 9.41

Hit# Of 5 Tentative ID MW MolForm CAS# Qual

1 Benzene-l,2,3,4-d4-, 5,6-dichlor... 150 C6D4C12 002199-69-1,91 2 1,4-Dichlorobenzene-d4 150 C6D4C12 003855-82-1 91 3 1,2-Dichlorobenzene-d4 $$ Benzen... 150 C6D4C12 002199-69-1 91 4 1,4-Dichlorobenzene-d4 150 C6D4Ci2 ____£02855jJB2j^l_2^ Abundance Scan 1221 (10.253 min): LBB0418.D (-) m/z 150.00 100.00% 1'iO

115 52 78 5000

'n/z-> Abundance Ol I"' ’ I" " I A 10 20 30 40 50 60 70 80 90 100110 120 130 140 150 160 #41699: Benzene-1,2,3,4-d4-, 5.6-dichloro- $$ 1,2-Dichloro... u 10.00 10.20 10.40 10.60 m/z 151.95 77.07%

1$0

115 ''"M tililil 52 78 10.00 10.20 10.40 10.60 m/z 115.10 60.73% 38 87 li ,1 I 124 0 I''''I m/z-> 10 20 30 40 50 60 70 80 90 100110 120 130 140 150 160 Abundance #41701:1.4-Dichlorobenzene-d4 150

10.00 10.20 10.40 10.60 Wgg 115 m/z 52.10 51.79%

52 78

28 fP 12 T-rrrrrrrt4ttr 0 ^ 99 Altai...... ' ” I" " I' m/z-> Abundance 10 20 30 40 50 60 70 80 90 100110 120 130 140150 160 #41700: 1,2-Dichlorobenzene-d4 $$ Benzene-1,2.3.4-d4-. 5,6... 1$0 ri 10.00 10.20 10.40 10.60 m/z 78.10 51.60%

5000 115 78 52

0 1'' ’ 'T 40 1 m/z-> 10 20 30 40 50 60 70 80 90 100110 120 130 140150 160 10.00 10.20 10.40 10.60

LBB0418.D 5080402BBC.M Mon Apr 22 18:37:39 2002 Page 3

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