GCMS analysis results for sample AD31638, Jan 28 2002

NYC 9/11 Public Portal Document Library searen compound Report

Data File : C:\MSDCHEM\1\5973N\02JAN17\31638.D vial: 5 Acq On : 17 Jan 2002 1:32 pm Operator: Sample : 508 scan Inst : Instrumen Mise : January 17, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\l..-\SCAN508.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 5 3-Cyanocarbazole $$ 9H-Carb... Concentration Rank 4

R.T. EstConc Area Relative to ISTD R.T.

22.28 0.14 ug/L 76442 Phenanthrene-dl0 22.63

Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 3-Cyanocarbazole $$ 9H-Carbazole... 192 C13H8N2 057102-93-9 64 2 N-perdeuteriobenzylideneaniline 192 C13D11N 000538-51-2 59 3 1,3-Benzodioxole, 4-methoxy-6-(2... 192 C11H12O3 000607-91-0 52 4 2-CYANOCARBAZOLE $$ 9H-Carbazole... 192 C13H8N2 057955-18-7 50 Abundance Scan 1656 (22.280 min): 31638.D (-) m/z 192.10 100.00% 192

5000

96 ----- _ 82 22.00 22.20 22.40 22.60

miz—> 0 mH 40 49 70 11/111171778.. n 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 ll m/z 96.00 16.31% Abundance #103424:3-Cyanocarbazole $$ 9H-Carbazole-3-carbonitrile (CAS 152

5000 ' • i ‘ ■ i • • ■ ■ i ■ • ■ ■ i ■ ■ ■ ■ 22.00 22.20 22.40 22.60 96 164 m/z 191.10 15.32% 138

miz—> 0 i. ,! .... ।.... । ., p . <, । ....।n 2030405060 70 8090 100 110 120 130 140 150 160 170 180 190 200 111gr I.../ Abundance #88409: N-perdeuteriobenzylideneaniline 192

22.00 22.20 22.40 22.60 5000 82 m/z 146.10 14.72% 54 110 30 I 94 160 0 nir........1 ‘ ■ i“ '11 “ ■ 11 1111111111111111111111111 ■ i > 11 ■ nr] ... ।....,.. .-i1 Tr miz--> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 Abundance #102624:1,3-Benzodioxole, 4-methoxy-6-(2-propenyl)- (CAS)... .............I 1A 1 1 I 1 1 1 1 ’ 1 1 ' 1 ■ 11 ' ’ ' 1 1512 22.00 22.20 22.40 22.60 m/z 193.10 14.52% 5000

91 165 103 119I 131ll_____147I 0 “ ■ । ■ i ‘ । ■ ■ ■ ■ ।। । ■ 11 • ■ i 17IL— ■ i • •. ‘ I" ’ ■ i" •. i ■ ■1 ■ i1"' i"' ■ i'1' ■ i1 IItTT miz—> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 22 00 22.20 22.40 22.60

31638.D SCAN508.M Tue Jan 22 08:37:03 2002 Page 7

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