GCMS analysis results for sample AD31673, Jan 28 2002

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Laboratory report showing GCMS analysis of sample AD31673 including unknown compounds and surrogate recovery data.

NYC-WTC_000050053–000050065

Folder label: “GCMS X 1/3/02 A 1/17/02”

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NYC 9/11 Public Portal Document Library searcn compound Report

Data File : C:\MSDCHEM\1\5973N\02JAN17\31673.D Vial: 8 ' Acq Oh : 17 Jan 2002 8:39 pm Operator: Sample : 508 scan Inst : Instrumen Mise : January 17, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1. . .\SCAN5 08. M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 5 3-Cyanocarbazole $$ 9H-Carb... Concentration Rank 5 R.T. EstConc Area Relative to ISTD R.T. 22.28 0.13 ug/L 73843 Phenanthrene-dl0 22.65 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 3-Cyanocarbazole $$ 9H-Carbazole... 192 C13H8N2 057102-93-9 72 2 2-CYANOCARBAZOLE $$ 9H-Carbazole... 192 C13H8N2 057955-18-7 72 3 Benzo[1,2-c:3,4-c]bis(isothiazol ... 192 C8H4N2S2 074960-05-7 64 4 Phenanthrene, 9-methyl- $$ 9-Met... 192 C15H12 000883-20-5 53 Abundance Scan 1656 (22,280 min): 31673.D (-) m/z 192.10 100.00% 1912

5000

82 96 146 160 ......... ......A,, 22.00 22.20 22.40 22.60

miz—> 40 49 66 , .1 1 0 | | | 111 1 ■ i'| ■ i i 11 i H 11 > i i । 1111 i 11 I "i 111 i i 11 11 i | i i > | । > ■ 111"Tp »-i 11 > i ■ i1" • i ■ 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 lh— m/z 96.10 14.81% Abundance #103424:3-Cyanocarbazole $$ 9H-Carbazo!e-3-carbonitri]e (CAS 102

5000 22.00 22.20 22.40 22.60 96 164 m/z 193.10 14.80% 138

m/z—> 0 •■i" i■■■■i■■■■i" i " i" mMMPTT 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 H 4-rrp-r

Abundance #103420:2-CYANOCARBAZOLE $$ 9H-Carbazole-2-carbonitrile (CAS 192 —————— 22.00 22.20 22.40 22.60 5000- m/z 146.00 13.88%

96 164 0 111-1111111111011110377109711111110933101E7-1TTTTTT . ................. ............. m/z—> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 Abundance #102104: Benzo[1,2-c:3,4-c]bis(isothiazole) $$ Benzo[1,2-c... MMA 192 22.00 22.20 22.40 22.60 m/z 160.10 11.35%

5000 45 148 57 69 82 96 121 165 h 0 .>। । I । I . . , . | II , U II I j . H , । . . . . । I . . . . | 1 . . . ) . ... l'“.... I.... ili.... ----- n/z—> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 22.00 22.20 22.40 22.60

31673.D SCAN508.M Tue Jan 22 08:37:34 2002 * Page 7

NYC-WTC_000050063

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GCMS analysis results for sample AD31631, Jan 28 2002 · Box DEP Box 28

NYC-WTC_000049916

Laboratory report showing GCMS analysis of sample AD31631 including unknown compounds and surrogate recovery data.

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