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GCMS analysis results for sample AD31673, Jan 28 2002

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Laboratory report showing GCMS analysis of sample AD31673 including unknown compounds and surrogate recovery data.

NYC-WTC_000050053–000050065

Folder label: “GCMS X 1/3/02 A 1/17/02

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Scanned page image, NYC-WTC_000050064
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NYC 9/11 Public Portal Document Library Search Compound Report Data File : C:\MSDCHEM\1\5973N\02JAN17\31673.D Vial: 8 Acq On : 17 Jan 2002 8:39 pm Operator: Sample : 508 scan Inst : Instrumen Mise : January 17, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\SCAN508.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 6 Anthracene-dlO- Concentration Rank 2 R.T. EstConc Area Relative to ISTD R.T. 22.77 0.32 ug/L 181159 Phenanthrene-dl0 22.65 Hit# Of 5 Tentative ID MW MolForm CAS# Qual

1 Anthracene-diO-. 188 C14D10 001719-06-8 86 2 Acridine-D9 188 C13D9N 000000-00-0 72 3 Acridine-D9 188 C13D9N 000000-00-0 72 4 Anthracene-D10 188 C14D10 000000-00-0 59 Abundance Scan 1699 (22.771 min): 31673.D (-) m/z 188.10 100.00% 188

5000

94 40 52 66 - 80 160 22.40 22.60 22.80 23.00 23.20 0 Tn-rn-.Til...,.,!. THp m/z 94.00 17.09% n/z-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #84502: Anthracene-d10- 1(18

5000 --------- 22.40 22.60 22.80 23.00 23.20 m/z 189.10 16.14% 66 80 94 160 Of -H----- m/z-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #85254: Acridine-D9 108

22.40 22.60 22.80 23.00 23.20 5000 m/z 184.10 11.23%

93

niz-> 30 Oh —ppmmmm—pmpp 66 80 I, 40 50 60 70 80 90 1(X) 110 120 130 140 150 160 170 180 190 158 ml Abundance #85255: Acrkiine-D9 . ! . . . . 1 . . rr-| , . , . | . , , , I . 118 22.40 22.60 22.80 23.00 23.20 m/ z 80.10 9.86% 5000

93 158 66 80

m/z—> 0 i ■ ■ ■ ■ i 132 H 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 . .. 4.... 22.40 22.60 22.80 23.00 23.20

31673.D SCAN508.M Tue Jan 22 08:37:34 2002 Page 8

NYC-WTC_000050064

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NYC-WTC_000050064Source: NYC Law Department, mirrored locally

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