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GCMS blank results for sample AE03509, March 28, 2002

Machine-extracted title · confidence 90%

Laboratory report documenting GCMS analysis of a method blank for sample AE03509 to verify analytical system cleanliness.

NYC-WTC_000037660–000037679

Folder label: “GCMS X 2/19/02 A 3/8/02

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Scanned page image, NYC-WTC_000037678
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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C: \MSDCHEM\1\5973N\02MAR08\03509.D Vial: 5 Acq On : 8 Mar 2002 1:57 pm Operator: Sample : 508 scan Inst : Instrumen Mise : March 8, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\HP022102.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 13 Anthracene-dlO- Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T.

22.77 0.29 ug/L 239727 Phenanthrene-dl0 22.63

Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Anthracene-dlO- 188 C14D10 001719-06-8 90 2 DECADEUTEROPHENANTHRENE $$ Phena.,, 188 C14D10 001517-22-2-87 3 Anthracene-D10 188 C14D10 000000-00-0 87 4 Acridine-D9 188 C13D9N 000000-00-0 86 Abundance Scan 1718 (22.768 min): 03509.D (-) m/z 188.10 100.00% 188

5000 ............................................ — 22.40 22.60 22.80 23.00 42 54 66 80 0- mR 111111 mPPPPPT -H TITTTH 34 132 146 160 U rn/z 189.10 14.16% miz-> 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #84502: Anthracene-d10- 1)18

5000 ----- 22.40 22.60 22.80 23.00 m/ z 94.00 12.23% 80 94 160 66 miz-> 0- TPPT TT —hp ‘ 1 TH 1B‘1111*11"011TTTTTTIT +180l U 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #84500: DECADEUTEROPHENANTHRENE $$ Phenanthrene-d10 188 ‘ I ‘ ' ' I 1 T 1 TCTTur)r 2240 22.60 22.80 23.00 5000 m/z 184.05 11.92% 80 94 158

miz-> 0- TIP TTII 66 TTHy TTTTf nPPmmmpm 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 —ll Abundance #84498: Anthracene-D10 ........... /.............................. 188 22.40 22.60 22.80 23.00 m/z 80.00 8.64%

5000 80 94 66 160 0-mmTT --------------------------------- H • ■ 1 I * * ‘ < I ‘ ‘ ‘ < I ‘ 1 * ‘ I ' » * » I * miz—> 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 22.40 22.60 22.80 23.00

03509.D HP022102.M Fri Mar 15 10:08:59 2002 Page 15

NYC-WTC_000037678

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NYC-WTC_000037678Source: NYC Law Department, mirrored locally

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