Laboratory report documenting GCMS analysis of a method blank for sample AE03509 to verify analytical system cleanliness.
NYC-WTC_000037660–000037679Folder label: “GCMS X 2/19/02 A 3/8/02”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document
Library Search Compound Report » Data File : C: \MSDCHEM\1\5973N\02MAR08\03509.D Vial: 5 Acq On : 8 Mar 2002 1:57 pm Operator: Sample : 508 scan Inst : Instrumen Mise : March 8, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\HP022102 .M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 12 4-METHOXY-.BETA.-METHYLCINN... Concentration Rank 6 R.T. EstConc Area Relative to ISTD R.T. 22.28 0.12 ug/L 103300 Phenant hrene-d10 22.63 Hit# of 5 Tentative ID MW MolForm CAS# Qual/
1 4-METHOXY-.BETA.-METHYLCINNAMIC ... 192 C11H1203 019169-94-9 72 2 N-perdeuteriobenzylideneaniline 192 C13D11N 000538-51-2 64 3 Thiocyanic acid, 2-benzothiazoly. .. 192 C8H4N2S2 006011-99-0 53 4 Anthracene, 2-methyl- (CAS) $$ 2... 192 C15H12 000613-12-7 53 Abundance Scan 1675 (22.283 min): 03509.D (-) m/z 192.00 100.00% 1512
5000
' * i • . 82 96 146 160 22.00 22.20 22.40 22.60 44 66 , i 118 - 0- TTUTTITTTTTTTTTTHIIWI ——— m/z 191.00 22.61% miz—> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 Abundance #102588:4-METHOXY-.BETA.-METHYLCINNAM1C ACID $$ 2-Butenoi... 1$2
108 - 5000 22.00 22.20 22.40 22.60 146 175 m/z 146.00 15.31% 0- “ I ‘ ' " I'' > • I " ' •! ’’711’117 ) ’ tt I "IIIIITT 1’111117111 ‘ ’ ’158 1’1211111111 H -rn-rr miz—> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 Abundance #88409: N-perdeuteriobenzylideneaniline 1112 P -A , , - 22.00 22.20 22.40 22.60 5000 82 m/z 193.10 13.02% 54 110
miz—> O' 30 hmmp •‘i■•••i■ mH 1 94 mm 160 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 1 Abundance #102098: Thiocyanic acid, 2-benzothiazoly! ester (CAS) $$... T-r-p-T-r-r-j-r-r ‘ I ' ' ' ‘ l‘ 192 22.00 22.20 22.40 22.60 m/z 96.00 10.66% 5000
12,8290 108 122 134 148 160 _•1 ______ ; ■ 0 TTTTTTTpm 1 ■ • ■ ■ । ■ i * ■ 1 • i • ■ miz—> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 22.00 22.20 22.40 22.60
03509.D HP022102.M Fri Mar 15 10:08:59 2002 Page 14
NYC-WTC_000037677
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NYC-WTC_000037635
Laboratory report documenting GCMS analysis of a method blank for sample AE03508 to verify analytical system cleanliness.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000037720
Laboratory report documenting GCMS analysis of a method blank for sample AE03612 to verify analytical system cleanliness.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000037680
Laboratory report documenting GCMS analysis of a method blank for sample AE03510 to verify analytical system cleanliness.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000037780
Gas chromatography-mass spectrometry analysis of sample AE03616 performed on 3/28/2002, detecting other unknown compounds with surrogate 2,4-DDD at 5.0 µg detection limit.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000037700
Laboratory report documenting GCMS analysis of a method blank for sample AE03611 to verify analytical system cleanliness.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000037740
Laboratory report documenting GCMS analysis of a method blank for sample AE03614 to verify analytical system cleanliness.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000037760
Laboratory report documenting GCMS analysis of a method blank for sample AE03615 to verify analytical system cleanliness.
1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000037800
Laboratory report detailing gas chromatography-mass spectrometry analysis of sample AE03617 conducted on March 28, 2002.
1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000010967
Gas chromatography-mass spectrometry analysis of sample AE02718 performed March 5, 2002, documenting other unknown compounds and surrogate 2,4-DDD recovery at 97 percent.
1 shared topics · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000004494
Multi-page laboratory data sheet containing sample analysis results and metadata for DEP GCMS records from January to February 2002.
1 shared topics · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000010027
GCMS laboratory results for sample AE01510 conducted on March 5, 2002, showing surrogate recovery and unknown compounds.
1 shared topics · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000009966
Analytical results for sample AE01508 analyzed via GCMS on March 4, 2002, including surrogate recovery data.
1 shared topics · similarity 0.997
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Laboratory report documenting GCMS analysis of a method blank for sample AE03508 to verify analytical system cleanliness.
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