GCMS analysis results for sample AE01638, March 2002

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GCMS laboratory results for sample AE01638 conducted on March 5, 2002, showing surrogate recovery and unknown compounds.

NYC-WTC_000010126–000010145

Folder label: “GCMS X 1/23/02 A 2/21/02”

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NYC 9/11 Public Portal Document

Library Search Compound Report .. Data File : C:\MSDCHEM\1\5973N\02FEB21\01638.D Vial: 7 Acq On : 21 Feb 2002 8:11 pm Operator: Sample : 508 scan Inst : Instrumen Mise : February 21, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\HP022102 .M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N. L ********************************************************************* Peak Number 10 4-METHOXY-.BETA.-METHYLCINN... Concentration Rank 4 R.T. EstConc Area Relative to ISTD R.T. 22.28 0.14 ug/L 114077 Phenanthrene-dl0 22.63 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 4-METHOXY-.BETA.-METHYLCINNAMIC ... 192 C11H1203 019169-94-9 72 2 l-amino-2-methyl-4-isopropyl-thi... 192 C5H13N4PS 107264-54-0 50 3 N-(2-methylprop-2-enyl)-2-nitrob. .. 192 C10H12N2O2 000000-00-0 46 4 Thiocyanic acid, 2-benzothiazoly... 192 C8H4N2S2 006011-99-0 45 Abundance Scan 1675 (22.283 min): 01638.D (-) m/z 192.00 100.00% 192

5000

96 146 160 ■ ■ i ■ ■ ■ ■ i

niz-> 43 70 8? 0 . . । .'|.. t. .. . ।. 11 . |. . 11 ) 1111 p I i p . —m 1 118 mmmp 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 I—— m/z 22.00 22.20 22.40 22.60 96.00 17.27% Abundance #102588:4-METHOXY-.BETA.-METHYLCINNAMIC ACID $$ 2-Butenoi... 192

108 — 5000 22.00 22.20 22.40 22.60 146 175 m/z 191.00 14.19% 0- ■i■i■ “ ■ i' " ■ i■ i1 “ ■ i ■ ■ i “ ■' i' “ ■ i • “ ‘ i ■ ■ • i ■ • ■ ■ i ■ • " i ■ Nunt t]r miz-> 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 Abundance #101918:1 -amino-2-methyl-4-isopropyl-thiotriazaphospholin... 159 192

22.00 22.20 22.40 22.60 5000 m/z 146.00 13.91%

144 177 0- “ i “'' i ■ " ■ i •1 “ i" “ i “ “ i “1 ‘11"11" " 11"' I" “ 11''111' “i" "fl ■ ■■ >i — m/z-> 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 Abundance #102494: N-(2-methyIprop-2-enyl)-2-nitrobenzenamine T 1**’ 1 U 192 22.00 22.20 22.40 22.60 77 151 m/z 193.00 10.98% 130 93 104 5000 119

177 0 "’91111113110372111111""TT ’t8T T-p-r T^ -n-p- TImPmWumpmuT — miz-s 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 22.00 22.20 22.40 22.60

01638.D HP022102.M Mon Feb 25 10:55:51 2002 Page 12

NYC-WTC_000010141

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